GCMS analysis results for sample AE06756, April 2002

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Data File C:\HPCHEM\l\DATA\APR1602\6756.D Vial : 12 Acq On 16 Apr 2002 11:59 pm Operator: Sample gc/ms scan 3/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M. (RTE Integrator) Title : 209 625/TCLP calibration table .Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 3

R.T. EstConc• Area Relative to ISTD R.T.

37.31 0.49 ug/1 43331 Perylene-dl2 37.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxa^, 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 25 2 EthanedioTc acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 22 3 3,6-Dio^-2,4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 16 4 2,6-Dii^thyl-3,4-bis(trimethylsilyl 311 C15H29NO2Si2 000000-00-0 12 Abundance Scan 3515 (37.313 min): 6756.D (-) m/z73700100.00% 73 147 221 aiiiiii 281 355 253 429 191 37.00 37.20 37.40 37.60 X.,7,1... . I III I I m/z 147.10 75.39% ""I""p I'' " I I 'I Ti/z-> 40 60 80 100120140160180200220240260280300320340360380400 420 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 7i3 147

281 5000 37.00 37.20 37.40 37.60

369 m/z 221.05 62.78% 207 I" " I' 1" I" " I ■ ^1® I. . L 338 I ■n/z-> 40 60 80 100120140160180200220240260280300320340360380400 420 Abundance #30580: Ethanedioic acid, bis(trimethylsilyl) ester 73 147

37.00 37.20 37.40 37.60 5000 m/z 281.00 37.97% 45 i 219 p ' I' 1" " I ‘' I" " I" p-rrrprrrT|- I" " I Tl/z-> 40 60 80 100120140160180200220240260280300320340360380400 420 • Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 147 2:>i 37.00 37.20 37.40 37.60 m/z 355.05 35.12% 73 5000 191 117 ....... ........ Il 71 Ti/z-> 40 60 80 100120140160180200220240260280300 320340360380400420 37.00 37.20 37.40 37.60

6756.D GCMS0412.M Wed Apr 17 12:04:05 2002 Page 2

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