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GCMS analysis results for sample AE06756, April 2002

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DEP laboratory report of GCMS analysis for sample AE06756 conducted on April 18, 2002.

NYC-WTC_000060522–000060532

Folder label: “GCMS X 3/21/02 A 4/16/02

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Scanned page image, NYC-WTC_000060529
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\APR1602\6756.D Vial: 12 Acq On 16,Apr 2002 11:59 pm Operator: Sample gc/ms scan 3/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 14.81 4.50 ug/1 794073 Naphthalene-d8 15.85 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasilo^ne, decamethyl- 370 C10H3005Si5 000541-02-6 2 Silane, [[4- [^ 2-bis[(trimethylsily 458 C20H42O4Si4 056114-62-6 3 Benzoic acidZ 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 38 4 N-(Trifluor/acetyl)-N,O,O',0'.'-tetr 553 C22H42F3NO4Si4 000000-00-0 38 Abundance Scan 1064 (14.812 min): 6756.D (-) m/z73/00100700% 713

5000 267 355

J ■R

45 108 133154 193 223 ^ , 14.40 14.60 14.80 15.00 15.20 I 293 323 'I m/z 355,.O5 51.03% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #51266: Cyclopentasiloxane, decamelhyl- 73

355 553 267 M 14.40 14.60 14.80 15.00 15.20 m/z 267.00 49.18%

nnZz-> 50 100 150 200 250 300 350 400 450 Abundance #74512: Silane, [[4-[1,2-bis((trimethylsilyl)oxy]ethyl]-1,2 3$5 I ' ’ ' ‘ I ' a 14,40 14.60 14.80 15.00 15.20 5000 73 m/z 356.05 18.77%

QR1 ............. 1 179 207 , ,251 ................... , , 443 nnfe-> Abundance 50

73 100 150 200 250 300 #51296: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy]-, trimet 350 355 400 4^ ... M.. . 14.40 14.60 14.80 15.00 15.20 m/z 267.90 13.20% 5000

147 267

71/Z-> 47 50 100 , I, 150 ” 200 250 1. 300 350 400 450 M 14.40 14.60 14.80 15.00 15.20

6756.D GCMS0412.M Wed Apr 17 12:04:04 2002 Page 1

NYC-WTC_000060529

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NYC-WTC_000060529Source: NYC Law Department, mirrored locally

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