GCMS analysis results for sample AE06424, April 23, 2002

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Library Search Compound Report Data File C:\HPCHEM\l\DATA\APR0405\6424.D Vial: 10 Acq On 5 Apr 2002 8:53 pm Operator: Sample gc/ms scan 3/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 14.85 0.42 ug/1 64695 Naphthalene-d8 15.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 (91 2 N- (Trifluoroacetyl)-0,0',0' ’-tris(t 481 C19H34F3NO4Si3 000000-00-0 38 3 Silane, [ [4-1,2-bis [ (trimethylsily 458 C20H42O4Si4 056114-62-6 38 4 N-(Trifluor/acetyl)-N,O,O',0'1-tetr 553 C22H42F3NO4Si4 000000-00-0 38 Abundance Scan 1068 (14.849 min): 6424.D (-) m/z 73.00 100.00% 73

267 355 5000

• 1 ! 1 ■' 1 ‘ ! 1 1 ■ ‘ I ‘ ‘ 45 14.60 14.80 15.00 15.20 ’ ■ i 1.1 .. 133154,193.223 44 323 1 m/z 355.05 54.48% miz-> 50 100 150 200 250 300 350 400 450 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 5000 267 , . .... M... 14.60 14.80 15.00 15.20 m/z 267.00 49.77%

■ ■ । 1227 S23 |........... miz-> 50 100 150 200 250 300 350 400 450 Abundance #58326: N-(Trifluoroacetyl)-O,O',O"-tris(trimethyIsilyi)no 73 ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i 1 ■ 355 14.60 14.80 15.00 15.20 5000 m/z 355.95 16.65%

vfz~> L .100 126147 45

50 ,193 265 , .. 376..... 150 200 250 300 350 400 450 481

Abundance #57393: Silane, [4-[1,2-bis[(trimethylsilyl)oxy]ethyI]-1.2 73 305 14.60 14.80 15.00 15.20 m/z 268.00 12.36% 5000

45 147 I 117, , | , 179 207... 281 L 443 ′ ‘I 1 ‘ ‘ * i. ‘ ‘ ‘ ' i ‘ 1 ‘ ■ i ■ ‘ n/z—> 50 100 150 200 250 300 350 400 450 14.60 14.80 15.00 15.20

6424.D GCMS0408.M Wed Apr 10 12:23:25 2002 Page 1

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