GCMS analytical results for sample AE03829, March 29, 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2202\3829.D Vial: 10 Acq On : 23 Mar 2002 2:58 am Operator: Sample : gc/ms scan 2/20 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************** * * * * ******************************* Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.87 0.56 ug/1 84849 Naphthalene-d8 15.90

Hit# of 5 entative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 91 2 N-(Triflu/racetyl)-0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 38 3 N-(Trifluoroacetyl)-O,O1,O''-tris(t 481 C19H34F3NO4Si3 000000-00-0 38 4 Benzoic/acid, 2,6-bis[(trimethylsi1 3 70 C16H30O4Si3 003782-85-2 33 Abundance Scan 1070 (14.866 min): 3829.D (-) m/z 73.00 ' 100.00% 73

267 355 5000- ,..... /........... 14.60 14.80 15.00 15.20 ; 45 ——— 133154 193,223 4 ■ i ■ Tr Trr 1Ir TTr r 1 1 323 , 1 , m/z 267.0,0 52.25% miz-> 50 100 150 200 250 300 350 400 450 500 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

.5000 267 355 4 ____14.60 14.80 15.00 15.20 m/z 355.0,5 49.47% । ' ■ । ...... 207, 1 323 m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #58807: N-(Trifluoracety!)-0.0.0--tris(trimethylsilyl)epin 73 355 14.60 14.80 15.00 15.20 5000 m/z 356.0,5 19.69% 45 ; . I 140 184 281 480 m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #58326: N-(Trifluoroacetyl)-O,O',O"-tris(trimethylsilyl)no ■

• • l ’ 73 14.60 14.80 15.00 15.20 355 m/z 268.00 13.86% 5000

45 Td | I, 126147 193 265 [ 376 481 ■ ' i m/z-> 50 100 150 200 250 300 350 400 450 500 14.60 14.80 15.00 15.20

3829.D GCMS0308.M Tue Mar 26 14:57:58 2002 Page 1

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