GCMS analysis results for sample AE06425, April 23, 2002

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\APR0405\6425.D Vial: 11 Acq On 5 Apr 2002 10:51 pm Operator: Sample gc/ms scan 3/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 14.84 0.26 ug/1 40496 Naphthalene-d8 15.88 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 000541-02-6 80) 370 C10H3005Si5 2 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H32O3Si3 068595-79-9 58 3 N- (Trifluoro. cetyl) -N,O,O’ ,0 ''-tetr 553 C22H42F3NO4Si4 000000-00-0 37 4 N-Methyladre .aline, tri-TMS 413 C19H39NO3Si3 000000-00-0 33 Abundance * Scan 1067 (14.844 min): 6425.D (-) m/z 73.00 100.00%| 73

5000 267 355 ■ ■ i ' ■ ' ‘ i • ■ ■ 1 i • • 14.60 14.80 15.00 15.20 45 j । ■ ‘i1 ■ . 154.193.1 323 |............................ m/z 267.00 45.57% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.60 14.80 15.00 15.20 m/z 355.05 42.20%l

'■ ■ 1T .2 100 150 200 250 323 J mfz-> 50 300 350 400 450 500 550 Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 i 1 1 ' 1 i 1 1 14.60 14.80 15.00 15.20 5000 267 m/z 356.05 19.86% 179 356

iz-> Abundance L 50 100 147

150 209 237, , 200 250 .312.1... 300 350 400 450 #60162: N-(Trifluoroacetyl)-N,O,O',O"-tetrakis(trimethylsi ■ ■ । 500 ‘ 550 । ■

■ ■ i ■ ■ ■ ■ i' ■ • i ■ ■ ‘ ■ i ‘ ■ 73 14.60 14.80 15.00 15.20 m/z 357.05 10.64 355 5000

45 - 147 193 267 538 ' ■ i ■ ■ ■ • i ■ • ■ ■ i ' 1 1 1 ‘ 1 1 1 1 1 1 m/z—> 50 100 150 200 250 3CO 350 400 450 500 550 14.60 14.80 15.00 15.20

6425.D GCMS0408.M Wed Apr 10 12:23:35 2002 Page 1

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