NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\APR16O2\6635.D Vial: 8
Acq On : 16 Apr 2002 8:03 pm Operator:
Sample : gc/ms scan 3/22 Inst : 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
14.82 1.80 ug/1 330642 Naphthalene-d8 15.84
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxaiie, decamethyl- 370 C10H3005Si5 000541-02-6
2 3,4-Dihydroxymaydelic acid, ethyl e 428 C19H36O5Si3 000000-00-0
3 Silane, [[4-[b<2-bis[(trimethylsily 458 C20H42O4Si4 056114-62-6 43
4 N-(Trifluoro^etyl)-N,O,O' ,0''-tetr 553 C22H42F3NO4Si4 000000-00-0 43
Abundance Scan 1064 (14.815 min): 6635.D (-) m/z73.00100.00%
73
267 355
5000
45 14.40 14.60 14.80 15.00 15.20
108 133154 193 223 293 ,323 , ...................
m/z 355.05 57.56%
■n/z-> 50 100 150 200 250 300 350 400
Abundance #51266: Cyclopentasiloxane, decamethyl-
73
355
267 ........ I [......
5000
14.40 14.60 14.80 15.00 15.20
m/z 267.00 52.19%
207 323
"T"
50 100 150 200 250 300 350 400
Abundance #55759: 3,4-Dihydroxymandelic acid, ethyl ester, tri-TMS
3$5
M ,
73 14.40 14.60 14.80 15.00 15.20
552 m/z 356.05 20.26%
............ 208 , , 251 , 281^........ 385 413
T"
■n/z-> 50 100 150 200 250 300 350 400
Abundance #74513: Silane, [[4-(1,2-bis[(trimethylsilyl)oxy]ethylJ-1,2 Li
1*^
31 5 14.40 14.60 14.80 15.00 15.20
m/z 268.00 13.89%
5000
73
45 ...... I ITO ^7 ,251, 281........ ....... 443 ■l\
' I r
mZz-> 50 100 150 200 250 300 350 400 14.40 14.60 14.80 15.00 15.20
6635.D GCMS0412.M Wed Apr 17 12:03:04 2002 Page 1
NYC-WTC_000060485
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