GCMS analysis results for sample AE06635, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File :.C:\HPCHEM\l\DATA\APR1602\6635.D Vial: 8 Acq On : 16 Apr 2002 8:03 pm Operator: Sample : gc/ms scan 3/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Propanedioic acid, hexyl-, die Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 33.28 2.22 ug/1 338271 Chrysene-dl2 33.64

Hit# of 5 . Tentative ID MW MolForm CAS# Qual

1 Propanedioy? acid, hexyl-, diethyl 244 C13H24O4 005398-10-7 38 2 Cyclohexa^, (1,1-dimethylpropyl) - 154 C11H22 031797-64-5 35 3 Hexane, ^3-dimethyl- 114 C8H18 000584-94-1 27 4 Hexane, 4,3,4-trimethyl- 128 C9H20 016747-31-2 27 Abundance Scan 3075 (33.277 min): 6635.D (-) “m/z SYTOO 100.00% 57 1 2 70 43

5000 83 239 256 T-r-T 97 33.00 33.20 33.40 33.60 143 J ^171 185 199 , I, , , J. I'''' I'' MM Uw m/z 112.10 94.04% ■n/z-> Abundance 20 40 60

7 100 120 140 160 180 200 220 240 260 80 #32687: Propanedioic acid, hexyl-, diethyl ester ft 70

5000 83 112 33.00 33,20 33.40 33.60 m/z 70.00 79.02% ......... 42 98 I ll 199 217 ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #11064: Cyclohexane, (1,1-dimethylpropyl)- 7b T 33.00 33.20 33.40 33.60 m/z 71.10 73.57% 27 125 A 83

J 97 ,1, 139 154 ■nZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #3097: Hexane, 2,3-dimethyl- 43 33.00 33.20 33.40 33.60 m/z 43.05 65.98% 70 5000

27 55 I ' ' I ' 85......... 114................................................................................... nfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 33.00 33.20 33.40 33.60

6635.D GCMS0412.M Wed Apr 17 12:03:05 2002 Page 2

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