GCMS analysis results for sample AE06633, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR16O2\6633.D Vial: 6 Acq On : 16 Apr 2002 6:05 pm Operator: Sample : gc/ms scan 3/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P •

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Propanedioic acid, hexyl-, die Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 33.27 0.50 ug/1 71818 Chrysene-dl2 33.64

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Propanedioic ^id, hexyl-, diethyl 244 C13H24O4 005398-10-7 37 2 1-Butanol, 3-i6ethyl-, carbonate (2: 202 C11H22O3 002050-95-5 27 3 Pentane, 2,y3,3-tetramethyl- 128 C9H20 007154-79-2 27 4 Nonadecane,/4-methyl- 282 C20H42 - 025117-27-5 16 Abundance Scan 3075 (33.274 min): 6633.D (-) m/z 57.00 100.00% 57 71 1 2 43

5000 83

239 257 33,00 33.20 33'40 33.60

Ti/z-> 20 40 60 80 100 120 140 160 180 200 129( 157 I 207 220 XX- 240 260 m/z 112.10 99.81% Abundance #32687; Propanedioic acid, hexyl-, diethyl ester 57

.. X.1 70

5000 83 112 33.00 33.20 33.40 33.60 m/z TIToX 88.18% 42 98 X-A 20 40 60 I

80 II I

100 ll

120 140 160 180 200 199 217 220 240 260 Abundance #23336:1-Butanol, 3-methyl-, carbonate (2:1)

43 70 I"" I /'V" A

33.00 33.20 33.40 33,60 5000 m/z 87.34% 55

27 I I „ . ,"'i, I , I, ■ ,, ,,, .................................. .. Tife-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #65115: Pentane, 2,2,3,3-tetramethyl- A 57 33.00 33.20 33.40 33.60 in/z 4X705 67.21% 43 71 253

Ti/z-> 27

20 i 40 X60 80 99 I ”3 100 120 140 160 180 200 220 240 260 | ... I.. I f, 11/XI 71 33.00 33.20 33.40 33.60

6633.D GCMS0412.M Wed Apr 17 12:02:13 2002 Page 2

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