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GC/MS calibration data for sample 28322, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018492–000018518

Folder label: “GCMS X 12/18/01 A 12/30/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\28322.D Vial: 62 Acq On : 30 Dec 2001 7:56 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 19 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

38.02 0.94 ug/1 227073 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 38 2 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 38 3 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 4 Mercaptoacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 28 Abundance Scan 3592 (38.021 min): 28322.D (-) m/z 73.00 100.00% 73

147 5000 221 281 355 T 1 ‘ ’ 1 I ‘ ‘ ' T T 37.60 37.80 38.00 38.20 38.40

m/z-> 96 119 191 TT Tp—r , rPm 44 50 100 150 4 200 250 253., L . f " T rm i”! 300 350 327 | 400 401 429 1 I I | I I T I | 1 1 450 m/z 146.95 56.68% Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147

5000 281 37.60 37.80 38.00 38.20 38.40 45 369 m/z 221.05 3 6.83% I , 1 i 1 ‘ ■ 1 I 1 1 1 1 i 1 1 117 . 297, , 249 m/z-> 50 100 150 200 250 ' 300 ' 350 ' 400450 ' Abundance #58871:1 -Monolinoeoyiglycerol trimethy’gily! ether 73 T T 207 37.60 37.80 38.00 38.20 38.40 5000 147 •I 34 103 281 I I 1 Il li L,r 395 T III — I I . 404 ‘ ‘ i ■ ■ ■ ■ i ■ m/z-> 50 100 150 ‘ 200 250 300 350 400 450 Abundance #71005: Ethanedioic acid, bis(trimethylsilyl) ester T T T T 73 37.60 37.80 38.00 38.20 38.40 m/z 355.0 16.42% 147 5000

45 I .I 117 190 219 ■ ‘i ■ • m/z-> 50 100 150 ’ ‘ 200 250 300 350 400 ’ ’ 450 ‘ 37.60 37.80 38.00 38.20 38.40

28322.D GCMS1126.M Wed Feb 06 12:57:06 2002 Page 19

NYC-WTC_000018516

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NYC-WTC_000018516Source: NYC Law Department, mirrored locally

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