DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2 502\30649.D Vial: 34 Acq On : 25 Jan 2002 9:55 pm Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 18 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

37.76 0.66 ug/1 256941 Perylene-dl2 36.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 3 84 C12H3604Si5 003555-47-3 38 2 1 -Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 38 3 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 32 4 Ethanedioic acid,bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 Abundance 73 Scan 3563 (37.757 min): 30649.D (-) m/z 72.95 100.00% 147 5000- 221 281 355 37.40 37.60 37.80 38.00 ' m/z-> ■ ■ 42) ’ 1 50 117 TTr Tfr — 100 150 200 19114444827 250 140142 300 350 400 450 500 550 m/z 147.10 60.82% Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147

5000 281 37.40 37.60 37.80 38.00 45 369 m/z 221.05 36.30% , J , 1, , 117 J , 207 249 .... [.......... m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #55671 1-Monolinoleoyiglyccrol irimethyistly ather 73 ■ | ‘ | ■ r 1 ■ I 1 i i > I’T । । TIT

207 37.40 37.60 37.80 38.00 5000 147 m/ z 281.00 18.72% 34 103 281 . .395. ,482 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73 37.40 37.60 37.80 38.00 m/z 355.05 15.44% 5000 147

i । 2^1 327 415 gig 581 114‘IIIJIIIIITII 1 1 i ' m/z-> 50 100 150 200 250 300 350 400 450 500 550 37.40 .37.60 37.80 38.00

30649.D GCMS1126.M Mon Jan 28 12:19:15 2002 Page 18

NYC-WTC_000004271