DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2502\30649.D Vial: 34 Acq On : 25 Jan 2002 9:55 pm Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 17 1-Monolinoleoylglycerol trimet Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

36.50 1.16 ug/1 454807 Perylene-dl2 36.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 38 2 Propanoic acid, 2-oxo-3-(trimethyls 232 C9H20O3Si2 055887-51-9 32 3 Ethanedioic acid,/bis(trimethylsily 234 C8H1804Si2 018294-04-7 32 4 1,2-Benzenedicarboxylic acid, bis(t 310 C14H2204Si2 002078-22-0 25 Abundance Scan 3426 (36.499 min): 30649.D (-) m/ Z 73.0,0 100.00% 73 147 5000 221 281 ■ ‘ ■ i ■ ■ ■ ■ i ' ■ ' 1 I 111 । । । । i 253, [ , 327, [ 401 429 36.20 36.40 36.60 36.80 41 96 117, ,1914. • i ■ ■ ■ ■ i ■ ■i 1 ' 1 1 r ■ ■1 t । । । TI——m m/z 147.00 54.81% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 1 1 i ■ 1 1114/. 36.20 36.40 36.60 36.80 34 103 m/z 221.05 34.98%

m/z-> 50 100 150 200 250 1 300 281

350 400 395 450 482

Abundance #30222: Propanoic acid. 2-ox0-3-ttrimethyisilyi)- trimethy 147 73 36.20 36.40 36.60 36.80 5000 m/Z 281.00 1 8.03% 45 217 117.... 189 |............................ 1 1 1 i miz-> 50 100 150 200 250 300 350 400 450 Abundance #71006: Ethanedioic acid, bis(trimethylsilyl) ester 7b 36.20 36.40 36.60 36.80 m/z 207.00 14.02% 147 5000-

45 1._ L 117 | 190-219 ' l ‘ T IBT m/z—> 50 100 150 200 250 300 350 400 450 36.20 36.40 36.60 36.80

30649.D GCMS1126.M Mon Jan 28 12:19:10 2002 Page 17

NYC-WTC_000004270