Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018492–000018518Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\28322.D Vial: 62 Acq On : 30 Dec 2001 7:56 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 20 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 18
R.T. EstConc Area Relative to ISTD R.T.
39.58 0.54 ug/1 130740 Perylene-d12 37.12
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 37 2 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 28 3 Dithioerythritol, tetrakis(trimethy 442 C16H4202S2Si4 000000-00-0 23 4 Silanamine, N-[2,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 14 Abundance Scan 3762 (39.581 min): 28322.D (-) m/ z 73.00 1 00.00% 73 147 5000 221 .... 281 355 39'20 39.40 39.60 39.80 40.00 429
miz-> 45 , ’2--327 — -PPT 150 200 250 300 350 400 450 500 550 m/z 147.00 69.41% 50 100 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147
5000 saa,apa-==--pnpp4paan 281 39.20 39.40 39.60 39.80 40.00 45 369 m/z 221.05 3 8.64%
miz-> J , , ■ 117 50 100 . .207 249, ...... .. 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-sopropoxy-1.1.1.7 7.7-hexamethyi-3.5,5-tnsttrim 73 • i ‘ k • • i ' 39.20 39.40 39.60 39.80 40.00 5000 147 221 281 327 415 t 519 561 miz-> 50 166 150 200 250 300 350 400 450 500 550 yAW WywA Abundance #56591: Dithioerythritol, tetrakis(tri methylsilyl)- 73 39.20 39.40 39.60 39.80 '40'ob m/z 355.05 18.19% 5000
m/z~> 45 ■ ■ । 50 — ,101 100 147 । | 173 150 221
n 1247 200 250 300 336 1
350 404 400 450 500 550 A A ' ■ i 1 ■ ‘ ' i ■ 39.20 39.40 39.60 39.80 40.00
28322.D GCMS1126.M Wed Feb 06 12:57:10 2002 Page 20
NYC-WTC_000018517
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NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036614
Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.996
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NYC-WTC_000018416
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