GC/MS calibration data for sample 28322, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\28322.D Vial: 62 Acq On : 30 Dec 2001 7:56 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 18 Ethanedioic acid, bis(trimethy Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

36.72 1.57 ug/1 378328 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 38 2 di-Xylitol, cyclic 2,3-(phenylboron 238 C11H15BO5 074793-46-7 27 3 N-Benzhydrylidene-1- (2,4,6-trimethy 343 C24H25NO 089839-57-6 27 4 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 23 Abundance Scan 3450 (36.717 mln): 28322.D (-) m/z 73

147 5000 221 281 355 -PFTYTP 36.40 36.60 36.80 37.00 43 I’r 96 117 „ . _FIT 191 ,[ —— ---+327, ,401 4?9, m/z-> 50 100 150 200 250 300 350 400 Abundance #71005: Ethanedioic acid, bis(trimethylsilyl) ester 73 147 5000 —. rp rerm , , I ’ M"7 36.40 36.60 36.80 37.00 45 m/z 221.05 3 3.25% I ।I 117 ''' 190 219 ' i 1 '■ ■ ■ i • ■ • • i ■ 1 ■ ■ i 1 ■ i • m/z-> 50 100 150 200 250 300 350 400 Abundance #31417: d-Xylitol, cyclic 2 3-fphenviboronate; 147 1 ■ • i ■ • ■ ■ i ■ ■ • • i • f ■ ■ i ■ ■ T 36.40 36.60 36.80 37.00 61 5000 m/z 281.00 18.78% 104 31 ; 177 207 238............. I m/z-> 50 100 ‘ ' 150 ' 200 250 ' 300' ' 350 400 “--A- - Abundance #48514: N-Benzhydrylldene-1-(2,4,6-trlmethylphenyl)ethylaml 147 36.40 36.60 36.80 37.00 m/z 207.00 16.62% 5000-

1182......... 312 343 ............ L ■ ■ i 1 • ■ 1 i ‘ 1 • • i ■ ' ■ ■ i 1 ■ ‘ ■ i m/z-> 50 100 150 200 250 300 350 400 36.40 36.60 36.80 37.00

28322.D GCMS1126.M Wed Feb 06 12:57:01 2002 Page 18

NYC-WTC_000018515