Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
NYC-WTC_000019130–000019152Folder label: “GCMS X 12/13/01 A 12/22/01 AND 12/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\DEC2701\30256.D Vial: 17 Acq On : 29 Dec 2001 2:47 pm Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Ethanedioic acid, bis(trimethy Concentration Rank 13
R.T. EstConc Area Relative to ISTD R.T.
36.72 0.80 ug/1 128274 Perylene-d12 37.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Ethanedioic < 5a, bis(trimethylsily 234 C8H1804Si2 018294-04-7 38 2 3-1 sopropoxy ,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 32 3 2-Propenoic < id, 2-[(trimethylsily 232 C9H20O3Si2 055191-13-4 32 4 Butanoic aci 3-methyl-2-oxo-, bis 260 CllH24O3Si2 072361-19-4 32 Abundance 9 Scan 3450 (36.718 min): 30256.D (-) m/z 73.00 100.00% 73 147 5000 221 281 355 117 1911 , . 325, 1 401 429 36.40 36.60 36.80 37.00 45 : — PII i 'rf 1" * 11*1" Par , r*tigm"t h1' ' ■ idi ■ trj ■ 1 I 'T^' m/z 147.00 56.81% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #71005: Ethanedioic acid, bis(trimethylsily!) ester 73 147 5000 -----=----====-=-4== 36.40 36.60 36.80 37.00 45 — m/z 221.05 34.30%
Mz-> 50 117 T 1 DTT i 150 100 i . 190 219 .......... 200 250 300 350 400 450 500 ' ‘ 550 ' Abundance #60503: 3-Isopropoxy-1,1,1,7.7,7-hexamethyl-3,5,5-trs(trm 73 / 36.40 36.60 36.80 37.00 5000 m/z 281.00 18.96% 147 221 281 327 415 519 561 m/z—> 50 100 150 200 250 300 350 ' 400 450 500 550 Abundance #70934:2-Propenoic add, 2-[(trimethylsilyl)oxy]-, trimeth ■ • i 1 ■ ■ ■ i • ■ ‘ ■ i ■ ' 1 ■ i 1 1 • ‘ i 1 147 36.40 36.60 36.80 37.00 73 m/z 354.95 17.13% 5000 45
m/z-> —4 50 99 100 150 217 — , — i[ r r। i , 200 250 300 350 400 450 500 550 .... i 36.40 36.60 36.80 37.00 1 ■ i ' 1 ■ ■ i
30256.D GCMS1126.M Wed Jan 02 10:25:17 2002 Page 15
NYC-WTC_000019151
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NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017675
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30251 conducted on January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036798
GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000019035
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NYC-WTC_000019036
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Reference analysis report for gas chromatography-mass spectrometry quantification of volatile organic compounds conducted on December 29, 2001.
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