Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
NYC-WTC_000023789–000023810Folder label: “GCMS X 5/9/02 A 5/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY2002\9676.D Vial: 10 Acq On : 20 May 2002 4:02 pm Operator: Sample : EXTRACTED 5/9 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 14 3-Isopropoxy-l, 1,1,7,7,7-hexam Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 32.20 0.99 ug/1 34877 Chrysene-dl2 33.57 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy-l,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 42 2 2-Hexenedioic acid, bis(trimethylsi 288 C12H24O4Si2 055494-10-5 25 3 4-Cyclohexene-1, 2-dicarboxylic acid 348 C14H25C104Si2 106450-29-7 17 4 Phosphori acid, 2-(methoxyimino)et 313 C9H24N05PSi2 055044-12-7 9 Abundance Scan 2964 (32.198 min): 9676.D (-) m/ z 73.10 100.00%| 73
5000 147 / 221 281 for 12 1 355 429 31.80 32.00 32.20 32.40 32.60 45 1 ‘‘i ’■ 1 ''1 i 1 1 _L /’i/* m/z 147.15 29.59% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73
- 5000 147 31.80 32,00 32.20 32.40 32.60 m/z 221.10 18.60% 221 281 327 415 ' ' ] ■ ' 1 1 I 1 ' 1 ' I ' ‘ ' 1 1 ' 4A1 11111 ... 519 561 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #407//: 2-Hexenedioic acid, bis(trimethylsilyl) ester, (E)- 73 .... 1 ■ ' i ■ ■ 1 ' i ■ ‘ 31.80 32.00 32.20 32.40 32.60 5000 m/ z 281.00 12.64%| 147 45 — — — 112 244 273 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #48996: 4-Cyclohexene-1,2-dicarboxylic acid, 4-chloro-, bis 73 31.80 32.00 32.20 32.40 32.60 m/z 355.10 9.58%
5000 147 117 186 230 258 333 1 * I 1 ' ' ' I 1 1 J ' ' ‘ m/z—> 50 100 150 200 250 300 350 400 450 500 550 31.80 32.00 32.20 32.40 32.60
9676.D GCMS0520.M Tue May 21 11:39:25 2002 Page 14
NYC-WTC_000023809
OCR can misread numbers and units. Confirm readings against the page image before using them.
Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000023649
Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038871
Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039497
Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005367
Laboratory report showing non-detectable results for nitrosamines and chlorinated solvents in GCMS blank.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047979
GCMS analysis report for sample AE05749 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013943
TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
Page similarity is temporarily unavailable or this page has no indexed vector.
Readers open these alongside this record — through an Ask answer, the same folder, or indexed similarity. Not a claim they are about the same event.
NYC-WTC_000023646
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000023647
Technical data file header page from a GCMS analysis run associated with the World Trade Center site in May 2002.
Filed in the same folder
NYC-WTC_000023649
Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.
Filed in the same folder
NYC-WTC_000023662
Laboratory report showing GC/MS calibration data for volatile organic compounds analyzed on May 20-21, 2002.
Filed in the same folder
NYC-WTC_000023666
Laboratory report showing GC/MS reference analysis for sample AE09676 with quantitative results for volatile organic compounds.
Filed in the same folder