NYC-WTC_000009619
Calibration table page listing internal standards and response factors for GCMS analysis.
Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Document / 16 pages
GCMS calibration analysis results, DEP Labs, Feb 2002
Machine-extracted title · confidence 100%Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
NYC-WTC_000009835–000009850Folder label: “GCMS X 1/22/02 A 2/22/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\FEB2102\472.D Vial: 6 Acq On : 21 Feb 2002 7:01 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
30.92 0.36 ug/1 22563 Chrysene-dl2 33.80
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 53 2 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 38 3 2-Hexenedioic acid, bis(trimethylsi 288 C12H24O4Si2 055494-10-5 17 4 2-Ethyl-3-trimethylsilyloxy(trimeth 276 C12H2803Si2 000000-00-0 17 Abundance Scan 2819 (30.919min): 472.D (-) i m/ z 73 .00.... 10 0.00% 73
5000 147 221 355 281
m/z-? Abundance 45 1—m50— 100 150 4H 200 250 300 I 429 --------------- 350 400 450 500 550 #60503: 3-isopropoxy-1,1,1,7,7,7-hexamethyi-3,5,5-tris(trim 30.60 30.80 31.00 31.20 m/z 147.00 38.56%
73
5000 ... I].... 147 30.60 30.80 31.00 31.20 221 281 397 A1c m/z 221." 22.34% ......... .............,........ |........| T...........415.............. 519 561 m/z-_ ___ 50 100. 150 200 250 300 350 400 450 500 550 Abundance 73
207 30.60 30.80 31.00 31.20 5000 147 m/z 354.95 15.87% 34 103 281 395 482 m/z-> 50. 100. 150__ 200 250 300 350__ 400. 450 .. 500.. 550. Abundance #40777: 2-Hexenedioic acid, bis(trimethylsilyij ester, (E)- 73 30.60 30.80 31.00 31.20 m/z 281.00 13.07% 5000- 147 45
J, | 112 ■ ‘ i ■ • • ' i • ' ' ■ i ' ■ ' ■ i ■ ■ 244 273 m/z~> 50 100 150 200 250 300 350 400 450 500 550 30.60 30.80 31.00 31.20
472.D GCMS0208.M Fri Feb 22 09:42:52 2002 Page 10
NYC-WTC_000009849
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NYC-WTC_000009849Source: NYC Law Department, mirrored locally
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