GCMS calibration analysis results, DEP Labs, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\472.D Vial: 6 Acq On : 21 Feb 2002 7:01 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

21.69 0.29 ug/1 28909 Acenaphthene-dl0 21.29

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic acid,/4-ethoxy-, ethyl este 194 C11H1403 023676-09-7 94 2 1,3-Cyclohexadiene-1-carboxylic aci 194 C12H18O2 035044-59-8 50 3 2-Methoxyphenylacetic acid, ethyl e 194 C11H14O3 000000-00-0 43 4 Phenol, 4 -fomyl carbonyl - 150 C8H603 000000-00-0 38 Abundance 7 Scan 1814 (21.693 min): 472D (-) m/z 12 0 .95 100. 0 0 % / 121 149 5000 138 194 65 93 166 39 50 | 21.40 21.60 21.80 22.00 76 | THH TIPWPTTPT m/z 149.00 55.02% F’r •*i•> m/z->___ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180.. 190 200 Abundance #69400: Benzoic acid, 4-ethoxy-, ethyl ester 121 149 5000 194 138 21.40 21.60 21.80 22.00 65 93 166 m/z 194.05 32.95% 50 YTT-rq-rr-rr-j-T m/z-?30 40 50 60 70 80 ■।•••■। 76 ।■I• H i ■ ■ ■ ■ i ■ ■ ■ ■ i “1 ■ i" “ i “ ■ ■ i ■ 90 100 110 120 130 140 150 160 170 180 190 200 “ i"

Abundance 107 121 ....... 1....... 21.40 21.60 21.80 22.00 5000 194 m/z 138.05 29.40% 149

77 135 165 179 m/z->___ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #21211: 2-Methoxyphenylacetic acid, ethyl ester 121 21.40 21.60 21.80 22.00 m/ z 64.95 19.94% 91 5000 194

1III****** 107 133— —— 148 165 1 1“I•• m/z~> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 21.40 211.60 21.80 22.00

472.D GCMS0208.M Fri Feb 22 09:42:29 2002 Page 5

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