Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
NYC-WTC_000039469–000039496Folder label: “GCMS X 3/19/02 A 4/17/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\APR1702\6430.D Vial: 6 Acq On : 17 Apr 2002 1:08 pm Operator: Sample : gc/ms scan 3/19 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 15
R.T. EstConc Area Relative to ISTD R.T. 21.56 0.73 ug/1 131476 Acenaphthene-dl0 21.14
Hit# of 5 Tentative ID MW MolForm CAS# Qu
1 Benzoic acid, 4-ethoxy-, ethyl este 194 C11H1403 023676-09-7(87 2 Phenol, 3-(1-methylethyl)- 136 C9H120 000618-45-1 38 3 Ethyl 3-hydroxybenzoate 166 C9H10O3 007781-98-8 37 4 Benzoic acid, 2-hydroxy-, phenyl es 214 C13H10O3 000118-55-8 35 Abundance Scan 1799 (21.557 min): 6430.D (-) m/z 120.95 100.00% 121
149 5000 194 --------- 65 93 166
mz-> 39 i r 1 ■' i ■ 20 40 4 60 1, L '' l1 11 1 I' " ' 11 ‘ TIIIT " I 223 '1 T' " 11 80 100 120 140 160 180 200 220 240 260 260 300 320 340 TIIETI 341 T-pn-n-p-r 21.20 21.40 21.60 21.80 m/z 149.00 53.72% Abundance #21260: Benzoic acid, 4-ethoxy-, ethyl ester 121
149 5000 21.20 21.40 21.60 21.80 194 m/z 194.05 34.78% 27 65 93 166 | TTTTTTTTITTTT ' TTTTT 111 ■ ■111 i ■' 1 111 ■1 ■ i' r • • • r 1 ‘11 1111' 1 1’1 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #65731: Phenol, 3-(1-methylethyl)- 121 T kl ■ ■ i 1 21.20 21.40 21 60 21.80 5000 m/z 137.95 25.93% 136 77 103 ... 51 | ).... L i''1' i1'' ■ i1r 1111',T1111 ■' I r ' • ■ i1'11 r 1 • ’ i ■ •111'1111 r 1 ■1 r * ‘ * i1 ‘ ■111 ■ ■' i m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 — ' — -............... I I Abundance #13943: Ethyl 3-hydroxybenzoate 121 21.20 21.40 21.60 21.80 m/z 64.95 16.35%
5000 93 65 138 166
m/z—> 20 । । I I । । i I ! i । I i r TITTTTTTTTTTTTTTTT
40 60 T.r1 TTIITnur 1’111 1111111",. (>.,, ।. 11. TTITT 80 100 120 140 160 180 200 220 240 260 280 300 320 340 k 21.20 21.40 21.60 21.80 IT
6430.D GCMS0412.M Thu Apr 18 09:09:26 2002 Page 9
NYC-WTC_000039484
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NYC-WTC_000039497
Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038871
Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039453
Laboratory report documenting GCMS blank analysis of sample AE06430 conducted on April 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023789
Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000039437
Department of Environmental Protection site log sheet for the World Trade Center area covering March and April 2002.
Filed in the same folder
NYC-WTC_000039438
Fragmented page from a GCMS record series dated April 2002 within DEP Box 23 archives.
Filed in the same folder
NYC-WTC_000039441
Calibration report for GCMS analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039445
Laboratory report documenting GCMS reference analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039453
Laboratory report documenting GCMS blank analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder