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GCMS analysis results for sample AE06430, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.

NYC-WTC_000039469–000039496

Folder label: “GCMS X 3/19/02 A 4/17/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1702\6430.D Vial: 6 Acq On : 17 Apr 2002 1:08 pm Operator: Sample : gc/ms scan 3/19 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Phenethylamine, N-methyl-.beta Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 23.32 1.67 ug/1 298993 Acenaphthene-dl0 21.14 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Phenethylamine, /N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 43 2 N- (Trifluoroacetyl) -N,O,O' ,0' ‘-tetr 553 C22H42F3NO4Si4 000000-00-0 43 3 Benzeneethanamine, N- (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 38 4 Benzoic acid, ,4-bis (trimethylsil 370 C16H30O4Si3 010586-16-0 38 Abundance Scan 1991 (23.320 min): 6430.D (-) m/ z 73.00 100.00%! 73

5000 355 147 221 281 1 1 I I I I I ] I 1 1 T I I I I I I I I—I—T 401 23.00 23.20 23.40 23.60 45 ■ ‘ 117 TI 191 ,i 249, TT 327 । A. . 4 m/z 355.05 43.45%l mz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 73

5000 355 • ■ i ■ 1 1 r i ■ T ' 11 1 । । । । > > i • f 23.00 23,20 23.40 23.60 44 m/z 147.00 30.71%l 1 , 147 193 267294 7 T, 1 Tdn ] I f TT[ I t I TT I I I [ I TT I TT I I I I TT I I ] I I I I I I J )—I—I—I—I—I—I—I—I—[—T miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(TrifIuoroacetyl)-N,O,O',O”-tetrakis(trimethylsi 73

355 23.00 23.20 23.40 23.60 5000 m/z 221.05 25.27%| |

45 L 147 193 267 538 1 1 i 1 1 T*1Omn——TT 1 ' i ‘ 1 ' 1 i 1 ' ' ' i r 1 ' ' i 1 1 1 1 i 1 1 mz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] ---------- 73 23.00 23.20 23.40 23.60 355 m/ z 281.00 18.55%| 5000

45 208 251 281 , 386 458 548 - 1 1 i ' ' ' T I ' 1 T < i. 1 1 TT i 4 1 1 1 f 1' ' T T i 1 T ' 1 i ' ' ' ' i ' ' ' ' i ' ' 1 ' i 1 ' ' 1 i ' 1 miz-> 50 100 150 200 250 300 350 400 450 500 550 23.00 23.20 23.40 23 60

6430.D GCMS0412.M Thu Apr 18 09:09:27 2002 Page 10

NYC-WTC_000039485

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NYC-WTC_000039485Source: NYC Law Department, mirrored locally

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