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GCMS analysis results for sample AE06449, April 2002

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Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.

NYC-WTC_000039497–000039521

Folder label: “GCMS X 3/19/02 A 4/17/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \HPCHEM\ 1 \DATA\APR1 702\6449.D Vial: 7 Acq On : 17 Apr 2002 2:06 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 8 Silane, [[4-[1,2-bis[(trimethy Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 23.33 1.19 ug/1 219818 Acenaphthene-dl0 21.15 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, [[4-[1,2-bis[(trimethylsily 458 C20H42O4Si4 056114-62-6 38 2 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 35 3 Phenethylamine,/N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 35 41,3,5,7-Tetraethyl-1-ethylbutoxysil442C14H3806S15 073420-30-1 35 Abundance Scan 1991 (23.326 min): 6449.D (-) m/z 73.00 100.00% 73

355 5000 147 221 281 401 23.00 23.20 23.40 23.60 45 117 191 i 249 t 327 1 1 i ' 1 1 t T 1 1 - m/z 355.05 57.32% ' ' i ' ' ' ' l 1 1 ' ' l ' 1 1 1 l 1 ' m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74513: Silane, [[4-[1,2-bis[(trimethylsilyl)oxy]ethyl]-1 ,2 355

73 5000 ■ ■ j ■ ■ ■ ■ । ■ < • • । ■ ■ • > । । । । 23.00 23.20 23.40 23.60 m/z 147.00 35.36% 45 147 | 179 207 251 281 443 1 'i *1—————— TI ' 1 1 1 1 ' T T I I I I I I 1 I J 1dI m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60339: Benzeneethanamine, N-[(pentafIuorophenyl)methylene] 73 355 1 1 1 ' II 1 । I 1 1 1 1 I 23.00 23.20 23.40 23.60 5000 m/z 221.05 29.29%

____ __________ 208 251 281 386 458 548 —————————— T*——— — ———————— miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74238: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 1 ■ i ' • * ■ । 1 । । । 1 ■ > 1 । 1 . . . । 355 23.00 23.20 23.40 23.60 73 m/z 281.00 24.29%l 5000 -

44 - 147 179 265 294 384 TTIO]m—Ong-—TTT ' 1 i 1 r 1 ' i ‘ ■ 1 ' i m/z—> 50 100 150 200 250 300 350 400 450 500 550 23.00 23.20 23.40 23.60

6449.D GCMS0412.M Thu Apr 18 09:10:50 2002 Page 8

NYC-WTC_000039511

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NYC-WTC_000039511Source: NYC Law Department, mirrored locally

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