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GCMS analysis results for sample AE02645, Mar 15, 2002

Machine-extracted title · confidence 90%

Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.

NYC-WTC_000005415–000005434

Folder label: “GCMS X 2/5/02 A 3/7/02

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Scanned page image, NYC-WTC_000005426
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR0702\2645.D Vial: 18 Acq On 8 Mar 2002 6:27 am Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

21.65 0.23 ug/1 44085 Acenaphthene-dl0 21.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic acid, -ethoxy-, ethyl este 194 C11H1403 023676-09-7.97 2 Ethylparaben 166 C9H10O3 000120-47-8 49 3 2-Methoxyphenylacetic acid, ethyl e 194 C11H1403 000000-00-0 43 4 Acetic acid (benzoylamino)hydroxy- 195 C9H9NO4 016555-77-4 38 Abundance Scan 1809 (21.652 min): 2645. D (-) ]’ m/z 120 .95 100.00% 121 ! 1 149 5000 194 65 ................. %................ 93 166 39 21.40 21.60 21.80 22.00 r m***m 223 1mumuOummmmOmOWOPPOT 341 m/z 149.00 55.48% m/z- 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #21260: Benzoic acid, 4-ethoxy-, ethyl ester 121

149 5000 21.40 21.60 21.80 22.00 194 65 93 166 : m/z 194.05 31.76% 27 1 TTTTT ' i'' ■ ■ i' ■ ■' i'1 ' ■ i'' ■ ■ i ■' ■' i'' ■' i1''' i''' ■ i'' ■ ■ i ■1 i ■1 ■ ■ i ■ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance 121 ................. .. ........................... 21.40 21.60 21.80 22.00 5000 m/z 137.95 26.68% 65 93 138 166

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #21211: 2-Methoxyphenylacetic acid, ethyl ester 121 21.40 21.60 21.80 22.00 m/z 64.95 20.19% 91 5000- 194

m/z-> i ‘ 20 ' i'11 ■ r ■' ■ i' 40 60 +196 I 148 165 । 11111111111101111‘0110011‘0171111**0-0*1‘_—OmOTITT 80 100 120 140 160 180 200 220 240 260 280 300 320 340 21.40 21.60 21.80 22.00

2645.D GCMS0208.M Wed Mar 13 14:54:21 2002 Page 5

NYC-WTC_000005426

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NYC-WTC_000005426Source: NYC Law Department, mirrored locally

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