Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
NYC-WTC_000036614–000036644Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C : \HPCHEM\1\DATA\JAN0802\29466 . D Vial: 6 Acq On 8 Jan 2002 5:14 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *********************************************** * * * * * * * * ************** Peak Number 8 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 17
R.T. EstConc Area Relative to ISTD R.T.
20.85 3.66 ug/1 1834770 Acenaphthene-dl0 20.40
Hit# of /5 Tentative ID MW MolForm CAS# Qual
1 Benzoic acid, 4-ethoxy-, ethyl este 194 C11H1403 023676-09-7 97 2 Methylparaben 152 C8H803 000099-76-3 38 3 Acetic acid, (benzoylamino)hydroxy- 195 C9H9N04 016555-77-4 38 4 Anisyl propionate 194 C11H1403 007549-33-9 38 'Abundance Scan 1722 (20.855 min): 29466.D (-) m/ z 120.95 100.00% 121
149 5000 - 194 . —........ -- 65 93 166 39 20.60 20.80 21.00 21.20 0- J . ■ ■ i • 53,1774109 I 133 I, 179 207 .......... 281 ' I ' * 1 ' I 1 1 m/z 14 9.00 49.54% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #69400: Benzoic acid, 4-ethoxy-, ethyl ester 121
149 5000 - 194 TTi rJ 20.60 20.80 21.00 21.20 65 93 166 m/z 194.05 29.62%
m/z-> 20 ............ 50 1 ■ ■ ■ i • ■ ■ ■ i ■ 40 60 77 80 100 120 140 160 180 200 220 240 260 280 Abundance #66909: Methylparaben 121 T ■ / 1 ' i 1 ' ' ■ i ' ■ 20.60 20.80 21 00 21.20 5000- 152 m/z 138.05 27.81% 65 93 46 j ■ ■ i ' ' ■ ' i 1 ■ TT-p-r-rv-p-<-rT-p .-r II11TTTUn r-p r "II", rT11UE1T111—rTET m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #21503: Acetic acid, (benzoylamino)hydroxy- i I"T 121 20.60 20.80 21.00 21.20 m/z 64.95 18.88% 195 5000 65 92 149 30 -PPPPP I 177 A -A.......... — m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 20.60 20.80 21.00 21.20
29466.D GCMS0103.M Wed Jan 09 16:16:33 2002 Page 8
NYC-WTC_000036631
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NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033974
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018287
Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
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NYC-WTC_000036491
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
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Laboratory calibration data sheet for GCMS analysis of organic compounds including nitrosamines and chlorobenzenes dated December 13, 2001.
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Laboratory report detailing GCMS calibration analysis for various organic compounds including nitrosamines and chlorobenzenes conducted on December 13, 2001.
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