Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
NYC-WTC_000036614–000036644Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C: \HPCHEM\1\DATA\JAN0802\29466.D Vial: 6 Acq On 8 Jan 2002 5:14 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 9 Benzeneethanamine, N-[(pentafl Concentration.Rank 10
R.T. EstConc Area Relative to ISTD R.T.
22.64 13.75 ug/1 10575000 Phenanthrene-dl0 24.81
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Benzeneeth namine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 35 2 N- (Trifluq acetyl)-0,0',O"-tris(tri 495 C20H36F3NO4S13 000000-00-0 25 3 Noradren. ine, tetra-TMS 457 C20H43NO3Si4 000000-00-0 25 4 N- (Trifl oroacetyl)-N,0,0',0'1-tetr 553 C22H42F3NO4Si4 000000-00-0 22 Abundance Scan 1917 (22.645 min): 29466.D (-) m/ z 73.00 100.00% 73
5000 147 355 221 401 281 । 45 22.40 22.60 22.80 23.00 0-+ — 117 191 1, 249 . 327 1 i . 441 m/z 355.05 30.74% mlz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355
5000 — 1 1 1 1 1 1 1 1 22.40 22.60 22.80 23.00 45 m/ z 14 7.00 29.63% ' I I ...... 208 251 281 , 386.......... 458............... 548 m/Z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58807: N-(Trifluoracetyl)-O,O'.O"-tris(trirnethylsilyl)epin 73 __________ rr. । . . । !| । . 355 ’ '1 1 1 22.40 22.60 22.80 23.00 5000 m/z 221.05 21.50%
45 I 140 184 281 480 • • ■ i • ■ ■ • i > miz—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #57357: Noradrenaline, tetra-TMS --------............... 73 22.40 22.60 22.80 23.00 m/z 281.10 15.80% 5000 102 355
45 147 | ................. ....... 442 ........... ■ --- -
m/z--> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00
29466.D GCMS0103 ,M Wed Jan 09 16:16:37 2002 Page 9
NYC-WTC_000036632
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NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033974
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018287
Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
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NYC-WTC_000036491
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
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