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← Document results/DEP Box 22/GCMS X 12/7/01 A 1/2/02
Document / 27 pages

GCMS analysis results for sample AD29522, Jan 2002

Machine-extracted title · confidence 100%

Quality reviewed GCMS data listing surrogate compounds and retention times from January 3, 2002.

NYC-WTC_000036752–000036778

Folder label: “GCMS X 12/7/01 A 1/2/02

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Scanned page image, NYC-WTC_000036763
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC3101\29522.D vial: 63 Acq On 3 Jan 2002 3:00 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 6 Benzeneethanamine, N-[(pentafl Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

22.79 9.69 ug/1 9863860 Phenanthrene-dl0 24.99

Hit# of 5 Ten tive ID MW MolForm CAS# Qual

1 Benzeneethanamine, N- [ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 35 2 N- (Trifluoroacetyl) -0,0' ,0' '-tris (t 481 C19H34F3NO4Si3 000000-00-0 35 3 N- (Trifluoracetyl) -0,0',O"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 25 4 Noradrenaline, tetra-TMS_____________ 457 C20H43NO3Si4 000000-00-0 25 'Abundance Scan 1933 (22.794 min): 29522.D (-) m/ z 73.0,0 100.00% 73

5000- 147 355 ------- 221 281 । ' ' 1 ■ । ■ 45 117 191 ,1 249. [ 327 401 ... 22.40 22.60 22.80 23.00 23.20 I 1 L 441 0 ' - 4 r 1I ' 1 m/z 355.00 30.15% m/z-> 50 100 150 200 250 300 350 400 500 450 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355

5000 22.40 22.60 22.80 23.00 2320 45 m/z 147.00 29.02% , J , .... 208 251 281 j 386 458 548 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58326: N-(Trifluproacetyb-0.0‘,0"-tris(trimethylsily!)no 73

355 Tmm A 22.40 22.60 22.80 23.00 23.20 5000- m/z 221.0,0 20.69%

45 i 120 147 193 265 481 miz-> 50 100 150 200 250 300 350 400 450 500 550 'Abundance #58807: N-(Trifludracetyl)-O,O',O"-tris(trimethylsilyl)epin ......... — A i ' ■ 73 22.40 22.60 22.80 23.00 23.20 355 m/z 281.05 15.60% 5000-

, 45L h 140 , 184.... 281 ..... 480 ' ■ i ’ ' 1 ■ i ' 1 r ’ i ' ■ ' ' i ' 1 ........................... ................... m/z—> 50 100 150 200 250 300 350 400 450 500 550 22.40 22,60 22.80 23.00 23.20

29522.D GCMS1126.M Fri Jan 18 16:48:31 2002 Page 6

NYC-WTC_000036763

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NYC-WTC_000036763Source: NYC Law Department, mirrored locally

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