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GC/MS calibration data for sample 30645, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018470–000018491

Folder label: “GCMS X 12/18/01 A 12/30/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30645.D Vial: 53 Acq On : 30 Dec 2001 10:14 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

21.03 1.17 ug/1 624036 Acenaphthene-dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzoic acid, 4-ethoxy-, ethyl este 194 C11H1403 023676-09-7 97 2 1-Cyclopentene-1 -propanoic acid, .b 168 C10H16O2 061833-30-5 80 3 Ethyl 3/nydroxybenzoate 166 C9H10O3 007781-98-8 38 4 ortho ydroxypropiophenone 150 C9H10O2 _______ 000610-99-1 38 Abundance Scan 1741 (21.028 mln): 30645.D (-) m/z 120.95 100.00% 121

149 5000 138 194 I ' • ■ ■ i ■ ■ ■ ■ i • ■ ■ ■ i • • ■ ‘ i ■ • ■ 39 93 166 20.60 20.80 21.00 21.20 21.40 I 50 I, 76 1 109 mpphpmmpmtt ‘I | 179 TTTgr " i •1 m/z 149.00 49.35% miz-s :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance> #21260: Benzoic acid, 4-ethoxy-, ethyl ester 121

149 5000 l • ■ ■ ■ I ■ TTTTTTT 138 20.60 20.80 21.00 21.20 21.40 194 65 93 166 m/z 138.0 28.73% 27 11111 * * 11111111111L111 * I 1 T TVIpugT • > l • ’ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #14561 1-Cyclopentene-1 -propanoic acid. .beta.-methyl-, me 58 79 95 121 8000 T T T T TT 20.60 20.80 21.00 21.20 21.40 109 6000 m/z 194.0 28.31% 4000 150 ........................... Il , | .... | ... I j . l . I ! ... 1| 1 I 1 I | 1 l iI . . . . | ..... I.......... ;...... 168............... |....( . ,.... | . . . . I . H . j H l . I . . . . I I . . . ( . . . , | .j.. miz-> :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #13943: Ethyl 3-hydroxybenzoate 121 T T p' < 1111 < 20.60 20.80 21.00 21.20 21.40 4 m/z 65.0 21.14% 5000 93 65 138 166 151 mMppummmmmmmmmmpmppm mWPMTDTTTT 1‘T p. TV. | I l I I I ■ I 1 (Torrrmmi m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 20.60 20.80 21.00 21.20 21.40

30645.D GCMS1126.M Fri Feb 01 10:53:01 2002 Page 8

NYC-WTC_000018482

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NYC-WTC_000018482Source: NYC Law Department, mirrored locally

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