GCMS analysis results for sample AD29563, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\29563.D Vial: 36 Acq On : 28 Dec 2001 11:11 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

21.04 0.57 ug/1 310776 Acenaphthene-dl0 20.57

Hit# of 5 Tentative III MW MolForm CAS# Qual

1 Benzoic acid, 4-ethoxy-, ethyl este 194 C11H1403 023676-09-7 96 2 Anisyl propionate • 194 C11H14O3 007549-33-9 43 3 1-Cyclopentene-1-propanoic acid, .b 168 C1OH1602 061833-30-5 42 4 Ethanone, 1- (4 ethoxyphenyl ) - 'Abundance C Scan 1743 (21.042 min): 29563.D (-) 121 164 C10H12O2 m/z 55 001676-63-7 40

5000 149 138 194 65 93 39 166 20.80 21.00 21.20 21.40 i 50 Ju ill 76 | 104 i. 207 .1 179 ■ r " ■ 11 "I1! ............. Hmm T TTT i1r m/z 14 9.00 49.87% m/z-> :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #21260: Benzoic acid, 4-ethoxy-, ethyl ester 121

149 / TYr 5000 T 20.80 21.00 21 20 21.40 138 194 — 65 93 166 m/z 137.95 31.33% 27 I TIUTTTTETTTT I r "' i"'' r " ■ i'" ‘ i p m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #21256: Anisyl propionate 121 t

20.80 21.00 21.20 21.40 5000- m/z 194.05 30.08% 91 194 77 I 109 TTTTTTTTTT TIETTT’TO-I’T_Iu"UEIB—EEII"ITT ■ r'" r " ■ i " ■' I"'' i" " i" " i m/z—> 20 30 40 50 60 70 80 90 100 110 120130 140 150160 170 180 190 200 210 'Abundance #14561:1-Cyclopentene-1-propanoic acid, .beta.-methyl-, me / i 58 79 95 121 20.80 21.00 21.20 21.40 8000 m/z 65.0 19.99% 109 6000

4000 150 168 ‘T l“ "I''" I l I •'••I "I"' i" "I '"I ""I । t i i i । i i .jr.r. । । । । । । T‘ ---------- TA miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 20.80 21.00 21.20 21.40

29563.D GCMS1126.M Tue Jan 08 11:42:29 2002 Page 6

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