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GCMS blank analysis results for sample AD30643, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.

NYC-WTC_000018420–000018435

Folder label: “GCMS X 12/18/01 A 12/30/01

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Scanned page image, NYC-WTC_000018431
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC27O1\LBE.D Vial: 51 Acq On : 30 Dec 2001 8:17 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

21.09 0.23 ug/1 93765 Acenaphthene-dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzoic acid, -ethoxy-, ethyl este 194 C11H14O31 023676-09-7 95 2 Anisyl propio: .te 194 C11H14031 007549-33-9 47 3 1-Cyclopentene-1 -propanoic acid, .b 168 C10H16O2! 061833-30-5 42 4 4-Methoxyphenylacetic acid ethyl es 194 C11H14O3> 014062-18-1 37 Abundance Scan 1748(21.091 min): LBE.D(-) m/z 120.95 100.00% 121 .................... /

5000 149 138 194

39, 50 s6 7684 93 193 166 20.80 21.00 21.20 21.40 m*nnmmmmmmmmmmmmmmm m/z 149.00 46.17% m/z-> :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #21260: Benzoic acid, 4-ethoxy-, ethyl ester 121

5000 138 149

194 mom 20.80 21.00 21.20 21.40

. . /V. 27 65 60 93 166 m/z 194.05 28.52%

m/z-> kmp :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #21256; Anisyl propionate 121

20.80 21.00 21.20 21.40 5000 m/z 138.05 24.42% .................... ................................ 77 91 194 138 I | 109 110*0mB—0mmnTna—mnmnn—npagrr miz-> :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance। #14561:1-Cycfopentene-1-propanoic acid, .beta.-methyl-, me 58 79 95 121 20.80 21.00 21.20 2140 8000 m/z 64.95 16.35% 109 6000

A.hasa 4000 150

m/z—> qmmmmmmmmaaaPm 168 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 20.80 21.00 21.20 21.40

LBE.D GCMS1126.M Fri Feb 01 11:31:55 2002 Page 6

NYC-WTC_000018431

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NYC-WTC_000018431Source: NYC Law Department, mirrored locally

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