Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
NYC-WTC_000018420–000018435Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\LBE.D vial: 51 Acq On : 30 Dec 2001 8:17 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 3-Isopropoxy- 1,1,1,7,7,7-hexam Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 20.27 0.93 ug/1 384830 Acenaphthene-dl0 20.56 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy-1,1, 1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 45 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 40 3 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 10 4 Heptadecanoic acid, trimethylsilyl 342 C20H4202Si 055517-58-3 9 Abundance Scan 1659 (20.274 mln): LBE.D (-) m/z 73.0,0 100.00% 73
5000 147 281
45 327 20.00 20,20 20.40 20.60 — ITT 117 191,221 249 1 t 383 415 ' ri T 1" ■ ‘I r । i i i“i f ih । i । i । i । । । i । । । । । m/z 147.00 34.39% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73
* 5000 147 20.00 20.20 20.40 20.60 221 281 m/z 281.00 31.70% 415 327,}2o** 519 561 m/z-> ’50 100 150 200 250 300 350 400 450 500 550 Abundance #52459; Trisiloxane, 1,1,1 5.5.5-hexametby-3,3-bisi{trimet 73 147 -- I■■ ■ 'I ' ' ' ' 1 ■ • ■ • l 281 20.00 20.20 20.40 20.60 5000 m/z 326.9,0 11.61% 369 207 249, 11. 1 338 1 •I’**+I1-**IS-**1**--I8+-*I*3*I-*-I**+-I-++IIIIS Trs 1 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #48317:4-Amino-5-imidazole carboxamide, tris(trimethylsily 1 • i • 1 T 73 20.00 20.20 20.40 20.60 m/z 74.00 8.80% 327 5000
LA 237 45 147 m/z—> I 172 212 ■ ■ I • 1 ■ ■ I 1 1 1 1 1 1 1 1 1 1 1 50 100 150 200 244 250 1 1 I *1 300 350 400 i________________________________ » । । » i r-j i < । i । i i i i । i i i—। । i i 450 500 550 11 I ' 1 1 1 I 20.00 20.20 20.40 20.60
LBE.D GCMS1126.M Fri Feb 01 11:31:50 2002 Page 5
NYC-WTC_000018430
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NYC-WTC_000018546
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019049
Laboratory report documenting gas chromatography-mass spectrometry blank analysis for volatile organic compounds conducted on January 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017663
Laboratory report documenting gas chromatography-mass spectrometry blank analysis conducted on December 27, 2001.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017126
Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034958
Calibration report showing recovery percentages for various chemical standards used in the GCMS analysis.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004149
Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036798
GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035776
Laboratory data sheet recording GCMS analysis of a blank sample for nitrosamines and chlorinated compounds.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031088
Gas chromatography-mass spectrometry analysis of environmental sample AD26202 conducted Dec 5, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.993
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NYC-WTC_000018416
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
Filed in the same folder
NYC-WTC_000018417
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
Filed in the same folder
NYC-WTC_000018436
Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
Filed in the same folder
NYC-WTC_000018440
Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
Filed in the same folder
NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
Filed in the same folder