Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
NYC-WTC_000018420–000018435Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\LBE.D Vial: 51 Acq On : 30 Dec 2001 8:17 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.
17.46 1.59 ug/1 637129 Naphthalene-d8 15.28 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 27 2 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 23 3 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 4 Silane, [1/2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 12 Abundance Scan 1352 (17.455 mln): LBE.D (-) m/z 73.00 1 00.00% 73
5000 341
45 147 429 17.20 17.40 17.60 17.80 m/z-> 0-m 117 [ 179.207 251 281 311 L i ....... 397...... L TTT TTTTTTTTTTTTTTTTTTTmITTTUTEET"TIT m/z 341.00 40 60 80 100120140160180200220240260280300320340360380400420 33.26% Abundance #56714:1,1,1,5,7,7,7-Heptemethyl-3,3-bls(trimethylsiloxy)t 73
147 5000 267 355 T 17.20 17.40 17.60 17.80 4 T ‘ l ‘ •
429 45 207 m/z 147.00 13.81% .....—I ODl—... Tr T TIUIB BT TTHT 1’*+’l+’’* Wpm] m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341 __ _____ ) V__________ *’1***I***1 ’’’’I44 17.20 17.40 17.60 17.80 429 5000 m/z 325.00 10.78% 147 207 267 311 TOCCmuu91m06—90—a—|B80888811 TgT Thpp Il 117 m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance 713 #48337:2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- 341 ’ • i r/ PmPPP 17.20 17.40 17.60 17.80 m/z 342.00 10.71% 5000- 45 91 | 116 146 227 269 31 _ /> TI Tp mopm TWTTmp TpTTTprrrpTrrpTTTpTrrjTT^^ > t । > i i i । i 8,88 * 1**
40 60 80 100120140160180200220240260280300320340360380400420 17.20 17.40 17.60 17.80
LBE.D GCMS1126.M Fri Feb 01 11:31:46 2002 Page 4
NYC-WTC_000018429
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NYC-WTC_000018546
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019049
Laboratory report documenting gas chromatography-mass spectrometry blank analysis for volatile organic compounds conducted on January 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017663
Laboratory report documenting gas chromatography-mass spectrometry blank analysis conducted on December 27, 2001.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017126
Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034958
Calibration report showing recovery percentages for various chemical standards used in the GCMS analysis.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004149
Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036798
GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035776
Laboratory data sheet recording GCMS analysis of a blank sample for nitrosamines and chlorinated compounds.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031088
Gas chromatography-mass spectrometry analysis of environmental sample AD26202 conducted Dec 5, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.993
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NYC-WTC_000018416
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
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NYC-WTC_000018417
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
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NYC-WTC_000018436
Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
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NYC-WTC_000018440
Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
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NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
Filed in the same folder