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GCMS blank analysis results for sample AD30643, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.

NYC-WTC_000018420–000018435

Folder label: “GCMS X 12/18/01 A 12/30/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\LBE.D Vial: 51 Acq On : 30 Dec 2001 8:17 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

17.46 1.59 ug/1 637129 Naphthalene-d8 15.28 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 27 2 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 23 3 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 4 Silane, [1/2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 12 Abundance Scan 1352 (17.455 mln): LBE.D (-) m/z 73.00 1 00.00% 73

5000 341

45 147 429 17.20 17.40 17.60 17.80 m/z-> 0-m 117 [ 179.207 251 281 311 L i ....... 397...... L TTT TTTTTTTTTTTTTTTTTTTmITTTUTEET"TIT m/z 341.00 40 60 80 100120140160180200220240260280300320340360380400420 33.26% Abundance #56714:1,1,1,5,7,7,7-Heptemethyl-3,3-bls(trimethylsiloxy)t 73

147 5000 267 355 T 17.20 17.40 17.60 17.80 4 T ‘ l ‘ •

429 45 207 m/z 147.00 13.81% .....—I ODl—... Tr T TIUIB BT TTHT 1’*+’l+’’* Wpm] m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341 __ _____ ) V__________ *’1***I***1 ’’’’I44 17.20 17.40 17.60 17.80 429 5000 m/z 325.00 10.78% 147 207 267 311 TOCCmuu91m06—90—a—|B80888811 TgT Thpp Il 117 m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance 713 #48337:2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- 341 ’ • i r/ PmPPP 17.20 17.40 17.60 17.80 m/z 342.00 10.71% 5000- 45 91 | 116 146 227 269 31 _ /> TI Tp mopm TWTTmp TpTTTprrrpTrrpTTTpTrrjTT^^ > t । > i i i । i 8,88 * 1**

40 60 80 100120140160180200220240260280300320340360380400420 17.20 17.40 17.60 17.80

LBE.D GCMS1126.M Fri Feb 01 11:31:46 2002 Page 4

NYC-WTC_000018429

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NYC-WTC_000018429Source: NYC Law Department, mirrored locally

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Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.994

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