Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
NYC-WTC_000018420–000018435Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\DEC2701\LBE.D Vial: 51 Acq On : 30 Dec 2001 8:17 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
14.31 1.31 ug/1 523718 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxa , decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Benzoic acid, 2 -bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 47 3 3,4-Dihydroxyb zyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 43 4 Benzoic acid, ,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 40 Abundance Scan 1009 (14.306 min): LBE.D (-) m/z 73.0.0 100.00% 73
5000 267 355 ----- 45 14.00 14.20 14.40 14.60 i , 1 88103118133 154 177 1932082233,21.. 293 .. 323339 “ ■ i ‘* i) • • n । i i. i jni• • r. । •. > • f. 1. > ।. .ri jT’j. n । • i11111 m/z 267.00 33.36% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 %
355 267 5000 14.00 14.20 14.40 14.60 m/z 355.0 24.70% i ■" ' i IT 11.» h ...»j • • • • । i "i“"i 191207 TTIut 2511 j . • • • 111 • • 11 i i T j i i i • j 323339 | miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73978: Benzoic acid, 2.5-bisttrimethylsiloxy)-, trimethyls 73 355 • I I I I I I l II J I I I I 1688* I 14.00 14.20 14.40 14.60 5000 m/z 356.05 9.55% 45 i I 147 179 207223 , I 370 MTTNI 267282297 TT j • 111J1111111111 11 1 11 I rrr J J J I I | I JI . । . t - j . । I । । . । । . j'. . । । i - । । . j mfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 - Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 14.00 14.20 14.40 14.60 m/z 74.0.0 8.54% 267 5000 179 356 45 147 1sl ।n »1,r। ii11>>>।*111111111>• । > 209 237 , 111i*i1111./j..v.।. | 312 341 L Dumuumwnunu TIIPITT m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.00 14.20 14.40 14.60
LBE.D GCMS1126.M Fri Feb 01 11:31:41 2002 Page 3
NYC-WTC_000018428
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NYC-WTC_000018546
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019049
Laboratory report documenting gas chromatography-mass spectrometry blank analysis for volatile organic compounds conducted on January 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017663
Laboratory report documenting gas chromatography-mass spectrometry blank analysis conducted on December 27, 2001.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017126
Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034958
Calibration report showing recovery percentages for various chemical standards used in the GCMS analysis.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004149
Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036798
GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035776
Laboratory data sheet recording GCMS analysis of a blank sample for nitrosamines and chlorinated compounds.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031088
Gas chromatography-mass spectrometry analysis of environmental sample AD26202 conducted Dec 5, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.993
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NYC-WTC_000018416
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
Filed in the same folder
NYC-WTC_000018417
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
Filed in the same folder
NYC-WTC_000018436
Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
Filed in the same folder
NYC-WTC_000018440
Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
Filed in the same folder
NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
Filed in the same folder