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GCMS blank analysis results for sample AD30643, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.

NYC-WTC_000018420–000018435

Folder label: “GCMS X 12/18/01 A 12/30/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\LBE.D Vial: 51 Acq On : 30 Dec 2001 8:17 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

14.31 1.31 ug/1 523718 Naphthalene-d8 15.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxa , decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Benzoic acid, 2 -bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 47 3 3,4-Dihydroxyb zyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 43 4 Benzoic acid, ,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 40 Abundance Scan 1009 (14.306 min): LBE.D (-) m/z 73.0.0 100.00% 73

5000 267 355 ----- 45 14.00 14.20 14.40 14.60 i , 1 88103118133 154 177 1932082233,21.. 293 .. 323339 “ ■ i ‘* i) • • n । i i. i jni• • r. । •. > • f. 1. > ।. .ri jT’j. n । • i11111 m/z 267.00 33.36% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 %

355 267 5000 14.00 14.20 14.40 14.60 m/z 355.0 24.70% i ■" ' i IT 11.» h ...»j • • • • । i "i“"i 191207 TTIut 2511 j . • • • 111 • • 11 i i T j i i i • j 323339 | miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73978: Benzoic acid, 2.5-bisttrimethylsiloxy)-, trimethyls 73 355 • I I I I I I l II J I I I I 1688* I 14.00 14.20 14.40 14.60 5000 m/z 356.05 9.55% 45 i I 147 179 207223 , I 370 MTTNI 267282297 TT j • 111J1111111111 11 1 11 I rrr J J J I I | I JI . । . t - j . । I । । . । । . j'. . । । i - । । . j mfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 - Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 14.00 14.20 14.40 14.60 m/z 74.0.0 8.54% 267 5000 179 356 45 147 1sl ।n »1,r। ii11>>>।*111111111>• । > 209 237 , 111i*i1111./j..v.।. | 312 341 L Dumuumwnunu TIIPITT m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.00 14.20 14.40 14.60

LBE.D GCMS1126.M Fri Feb 01 11:31:41 2002 Page 3

NYC-WTC_000018428

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NYC-WTC_000018428Source: NYC Law Department, mirrored locally

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