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GCMS blank analysis results for sample AD30643, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.

NYC-WTC_000018420–000018435

Folder label: “GCMS X 12/18/01 A 12/30/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\LBE.D Vial: 51 Acq On : 30 Dec 2001 8:17 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 11.13 0.97 ug/1 309706 1,4-Dichlorobenzene-d4 11.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H2404Si4 000556-67-2 87 2 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 28 3 6,7-Benzo- phenothiazine -5,5-dioxide 281 C16H11NO2S 000000-00-0 9 4 Benzene, 1 -phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 Abundance 4 Scan 663 (11.130 mln): LBE.D (-) m/z 281.0p 100.00% 211

5000

‘840411** P * ’ 1 I 'r* 1 ‘ l' 73 89 103 119 133 147 163 177 193 207 221 235 249 285 10.80 11.00 11.20 11.40 45 59 TTtm • I * • ’1,. I ■■■t । i । Tin "I rri Tssras r ■ r'/h । rt ■ . f, ■ ■ ■■ । । "r . । 1 . ■ m/z 282.0p 30.87% mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 2111

5000 - 10.80 11.00 11.20 11.40 133 m/z 283.op 17.32% 73 163 177 191 T 235 249 265 I ‘ 1‘4**1***1‘+‘41‘‘*‘I‘*‘*I****I‘**‘I‘*‘‘1*-**I‘**‘I" • • * i • • ■ • p ■ miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39624; 3.6-Bis(N-dimethylamino)-9-ethylcarbazole 281 T / k l 1‘* , l ‘ ’ I 10.80 11.00 11.20 11.40 5000 m/z 192.9p 12.69% 266

miz—> 1.40...... .1 ........ 222 23720. ' “60 ' 80 166 120 140 160 * 180 200 220 240 260 '11 P' 280 Abundance #39602:6,7-Benzo-phenothiazine-5,5-dioxide / • * I * • < । • ■ ■ i • ■ • ' i 281 10.80 11.00 11.20 11.40 m/z 133.00 10.71% 5000

217 232 m/z—> .1 118.199.294.4 ..M .252264, ■ . 40 60 80 100 120 140 160 180 200 ‘226’ ‘246' 260 280 T / \ I ‘ f • • I T T 10.80 11.00 11.20 11,40

LBE.D GCMS1126.M Fri Feb 01 11:31:36 2002 Page 2

NYC-WTC_000018427

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NYC-WTC_000018427Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004149

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.994

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