NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\LBE.D Vial: 51
Acq On : 30 Dec 2001 8:17 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209
Mise : Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
11.13 0.97 ug/1 309706 1,4-Dichlorobenzene-d4 11.67
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclotetrasiloxane, octamethyl- 296 C8H2404Si4 000556-67-2 87
2 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 28
3 6,7-Benzo- phenothiazine -5,5-dioxide 281 C16H11NO2S 000000-00-0 9
4 Benzene, 1 -phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9
Abundance 4 Scan 663 (11.130 mln): LBE.D (-) m/z 281.0p 100.00%
211
5000
‘840411** P * ’ 1 I 'r* 1 ‘ l'
73 89 103 119 133 147 163 177 193 207 221 235 249 285 10.80 11.00 11.20 11.40
45 59
TTtm • I * • ’1,. I ■■■t । i । Tin "I rri Tssras r ■ r'/h । rt ■ . f, ■ ■ ■■ । । "r . । 1 . ■ m/z 282.0p 30.87%
mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280
Abundance #41966: Cyclotetrasiloxane, octamethyl-
2111
5000 -
10.80 11.00 11.20 11.40
133
m/z 283.op 17.32%
73 163 177 191 T 235 249 265
I
‘ 1‘4**1***1‘+‘41‘‘*‘I‘*‘*I****I‘**‘I‘*‘‘1*-**I‘**‘I" • • * i • • ■ • p ■
miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280
Abundance #39624; 3.6-Bis(N-dimethylamino)-9-ethylcarbazole
281
T
/ k
l 1‘* , l ‘ ’ I
10.80 11.00 11.20 11.40
5000 m/z 192.9p 12.69%
266
miz—>
1.40...... .1 ........ 222 23720.
' “60 ' 80 166 120 140 160 * 180 200 220 240 260 '11 P'
280
Abundance #39602:6,7-Benzo-phenothiazine-5,5-dioxide /
• * I * • < । • ■ ■ i • ■ • ' i
281 10.80 11.00 11.20 11.40
m/z 133.00 10.71%
5000
217 232
m/z—>
.1 118.199.294.4 ..M .252264, ■ .
40 60 80 100 120 140 160 180 200 ‘226’ ‘246' 260 280 T
/ \
I ‘ f • • I T T
10.80 11.00 11.20 11,40
LBE.D GCMS1126.M Fri Feb 01 11:31:36 2002 Page 2
NYC-WTC_000018427
OCR can misread numbers and units. Confirm readings against the page image before using them.