Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
NYC-WTC_000018624–000018639Folder label: “GCMS X 12/19/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C: \HPCHEM\ 1 \DATA\DEC3101\30904.D Vial: 44 Acq On 2 Jan 2002 6:35 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,1,1,5,7,7,7-Heptamethyl -3,3- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 17.45 1.90 ug/1 555536 Naphthalene-d8 15.28 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,1,1,5,7,7,7-Henfamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 27 2 Cyclohexasiloxane, dodecamethyl- 444 C12H36O6Si6 000540-97-6 23 3 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 4 Silane, Abundance [1,2,3-benzenetriyltris(oxy342C15H3003Si3 Scan 1352 (17.454 min): 30904.D (-) 017864-23-2 22 m/z 73.00 100.00% 73
5000 341 147 45 lT 117 [ TOT TTTDuaamtd179 207225 251 —281 ’u1—15hmm mmLOB0311 ( ’tuT ....... 397......429 L 17.20 17.40 17.60 17.80 !.... ।. । n r 111 n । ] i m/z 341.00 28.31% miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714:1,1,1,5,7.7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 147 5000 267 ■ ■ i ‘ ' • • i • • 355 429 17.20 17.40 17.60 17.80 45 207 m/z 147.00 14.63% I I nphm PO]]mmpmmmmppmmpp T’T m/z-> Abundance T* 40 60 80 100120140160180200220240260280300320340360380400420 #56711: Cyclohexasiloxane, dodeca methyl- 73 341 — T 18.8 17.20 17.40 17.60 17.80 429 5000 m/z 325.00 9.43% 147 117 | 207 267 311 , , | । ।. > i > ।.... t।'I।।।। j > >> ■ I’ll 11 fh 111111111111111 n 11A111 miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48337:2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- **I*aAII"II7IIIIIIIII 73 341 17.20 17.40 17.60 17.80 rn/z 342.00 9.17% 5000 45 91 .................................. ................ . 40 60 80 100120140160180 2(X) 220 240 260 280 300 320 340 360 380 400 420 ' T 1 1 1 ' ' ‘ I ‘ ‘ m/z—> 17.20 17.40 17.60 17.80
30904.D GCMS1126.M Fri Jan 25 11:29:51 2002 Page 4 NYC-WTC_000018634
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NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018650
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30906 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018093
Automated laboratory log recording GCMS analysis of sample AD30694 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018005
Laboratory report listing PAHs and phthalates in a water sample scheduled for re-extraction and re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036842
GCMS analysis report for sample AD29670 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018576
Single-page document containing GCMS data or metadata associated with the WTC site in early January 2002.
Filed in the same folder
NYC-WTC_000018577
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
Filed in the same folder
NYC-WTC_000018579
Laboratory report documenting GCMS calibration data for sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018583
Laboratory report documenting GCMS reference analysis of sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018588
Laboratory report showing non-detect results for volatile organic compounds in a GC/MS blank sample.
Filed in the same folder