Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
NYC-WTC_000017703–000017723Folder label: “GCMS X 12/13/01 A 12/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C: \HPCHEM\ 1 \DATA\DEC2 701\30425.D Vial: 5 Acq On : 27 Dec 2001 3:04 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
20.27 2.76 ug/1 1172960 Acenaphthene-dl0 20.56
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3 - Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 45 2 Trisiloxane, 1,1,1,5,5,5 -hexamethyl 384 C12H36O4S15 003555-47-3 42 3 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 22 4 Octadecanoic acid, 2-[(trimethylsil 386 C22H46O3Si 056196-58-8 10 Abundance Scan 1659 (20.272 min): 30425.D (-) m/z 73.0,0 100.00% 73
5000 147 281 327 20.00 20.20 20'40 20.60 - 45 117. । 191271 251 . 1 355 383,415. m/z 147.00 35.32% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73
5000 147 20.00 20.20 20.40 20.60 221 281 m/z 281.00 31.68% 327 415 519 561 ' T1 1 rr ] » «• i i । »-r r • f > ■ *> h 1 ■ TTpanmBBTs m/Z~> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459; Trisiloxane, 1,1.1.5.5,5-hexamethyl-3,3-bis[(trimet 73 147 — 281 20.00 20.20 20.40 20.60 5000 m/z 326.90 12.24%
207 369 249, I 338 1 1111* * p-> । Tu ■ । i | Tit I ‘* 11* n > | । । * I j । i i i J i i i * [ « i i » i * ‘ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #48317:4-Amino-5-imidazole carboxamide, tris(trimethylsily 73 20.00 20.20 20.40 20.60 m/z 282.00 9.38% 327 5000 237 45 147 11 I 111 1 I I 172 212 1 । ‘T ' i'‘ ‘ | 'i ri f»—» 4*1*4*1*‘}‘*‘}****17‘‘I** .1 । 1 । miz-> 50 100 150 200 250 300 350 400 450 500 550 20.00 20.20 20.40 20.60
30425.D GCMS1126.M Wed Jan 02 11:04:04 2002 Page 6
NYC-WTC_000017715
OCR can misread numbers and units. Confirm readings against the page image before using them.
Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017675
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30251 conducted on January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
Page similarity is temporarily unavailable or this page has no indexed vector.
Readers open these alongside this record — through an Ask answer, the same folder, or indexed similarity. Not a claim they are about the same event.
NYC-WTC_000017649
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
Filed in the same folder
NYC-WTC_000017650
Laboratory log recording extraction parameters and sample counts for environmental samples processed in December 2001.
Filed in the same folder
NYC-WTC_000017654
Document showing calibration results for GCMS analysis of volatile organic compounds on December 27, 2001.
Filed in the same folder
NYC-WTC_000017658
Laboratory report documenting gas chromatography-mass spectrometry reference material analysis conducted on December 31, 2001.
Filed in the same folder
NYC-WTC_000017663
Laboratory report documenting gas chromatography-mass spectrometry blank analysis conducted on December 27, 2001.
Filed in the same folder