Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\DEC2701\30707.D Vial: 41 Acq On : 29 Dec 2001 10:35 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
20.28 6.71 ug/1 3916550 Acenaphthene-dl0 20.56
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy-1/ 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 38 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 37 3 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 10 4 Phosphoric acid, 3-(ethoxyimino)-2- 429 C14H36NO6PSi3 055334-96-8 10 Abundance ' Scan 1659 (20,277 min): 30707.D (-) m/z 73.00 1 00.00% 73
5000 147 281 327 20.00 20.20 20.40 20.60 45 1 0— ’ I 1 1 r'' | ' TIT 117 191,221 251 . 355.383 415. m/z 147.00 36.88% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73
5000 147 20.00 20.20 20.40 20.60 1 221 m/ z 281.00 35.14% 281 327 415..... 519 , 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane 1.1.1,5.5.5-hexamethy!-3,3-bisl(trimet 73 147 - 281 20.00 20.20 20.40 20.60 5000 m/z 326.90 14.33%
207 369 249 ,1.338 ........ .. . a.. I m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #48317:4-Amino-5-imidazole carboxamide, tris(trimethylsily 1 73 20.00 20.20 20.40 20.60 I m/z 282.00 10.23% 327 5000 237 45
1 1 i 1 1 ..... 147172 212 1 ■ ■ i r • J....... miz—> 50 100 150 200250 300 350 400 450 500 550 20.00 20.20 20.40 20.60
30707.D GCMS1126.M Mon Jan 28 11:24:06 2002 Page 6
NYC-WTC_000004448
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
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