Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
NYC-WTC_000018262–000018285Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30985.D vial: 39 Acq On 2 Jan 2002 1:45 am Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
20.27 6.73 ug/1 2484290 Acenaphthene-dl0 20.56
Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 S-Isopropox^l, 1,1,7,7,7-hexamethyl 576 C18H5207S17 071579-69-6 45 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H36O4S15 003555-47-3 37 3 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 12 4 Heptadecanoic acid, trimethylsilyl 342 C20H42O2Si 055517-58-3 9 Abundance Scan 1659 (20.272 min): 30985.D (-) m/ z 73.0,0 100.00% 73
5000 147 281 20.00 20.20 20.40 20.60
miz-> 45 117 , 0- —P 50 191 221 251 191,221251 m 100 .34,55,383,415.,/ ...... .......... 150 200 250 300 350 400 450 500 550 m/z 147.00 34.96% Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3.5,5-trls(trim 73
5000 147 20.00 20.20 20.40 20.60 221 281 20= A46 m/z 281.0.0 30.22%
miz-> ---9 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1.1,5,5,5-hexamethy-3.3-bis[(trimet 73 147 281 20.00 20.20 20.40 20.60 5000 m/z 326.90 11.34% 369 207 249, j 338 ! m/z-> 50 100 150 200 250 300 350 400 ' ' 450 500 550 Abundance #48317:4-Amino-5-imidazole carboxamide, tris(trimethylsily 73 20.00 20.20 20.40 20.60 m/z 282.00 8.64% 327 5000 237 45 147. I 172 212 1 ----- TIdr ' 50 ■ ■ < • • • ' i 1 ‘ ' i ■ m/z—> 100 150 200 250 300 350 400 450 500 550 20.00 20.20 20.40 20.60
30985.D GCMS1126.M Wed Jan 23 08:57:25 2002 Page 6
NYC-WTC_000018274
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NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017380
Laboratory report documenting GCMS analysis of sample AD31018 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder