Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
NYC-WTC_000018155–000018173Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\DEC3101\30713.D Vial: 28 Acq On 1 Jan 2002 3:07 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
20.28 1.93 ug/1 762328 Acenaphthene-dl0 20.56
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy-1,1.1, 7,7,7-hexamethyl 576 C18H5207S17 071579-69-6 45 2 Trisiloxane, 1,1, 1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 43 3 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 16 4 Octadecanoic acid, 2-[(trimethylsil 386 C22H46O3Si 056196-58-8 10 Abundance Scan 1659 (20.277 min): 30713.D (-) m/z 73.0,0 100.00% 73
5000 147 281
45 327 20.00 20.20 20.40 20.60 . ,-| 1 1 1 -Pin . , ■191 mr117 r 221 251 191-1 . i Birin 300 383 415 . 350 ' 400 450 500 550 m/z 147.00 34.97% m/z-> 50 100 150 200 250 'Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73
5000 147 1 20.00 20.20 20.40 20.60
221 281 35= 34E m/z 281.00 32.45% । j 347, 415 519 561 ThInnnnn—B—n—nmnn0—a—n/n—/nn——0/n/mB/md//n/3/B/n/T miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459; Trisiloxane, 1,1,1.5,5,5-hexamethyl-3.3-bis[(trirnet 73 147 . ... 281 20.00 20.20 20.40 20.60 5000 m/z 326.90 12.98%
369 207 249 338 i m/z-> &o‘ 100 150 1 200 250 300 350 400 450 500 550 Abundance #48317:4-Amino-5-imidazole carboxamide, tris(trimethylsily 73 20.00 20.20 20.40 20.60 m/z 282.00 8.94% 327 5000 237 45 147 । 172 212 i * ‘ I ‘ ‘ I• T-r-j-i-r ■ ।1 ■ ■ ■ j ■ ■ • ■) * ■ ■ ■ । ■ ■ • ■ । ■ • • i • * * * n * miz-> 50 100 150 200 250 300 350 400 450 500 550 20.00 20.20 20.40 20.60
30713.D GCMS1126.M Wed Jan 23 08:46:37 2002 Page 5
NYC-WTC_000018166
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NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder