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GCMS analysis results for sample AD30985, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.

NYC-WTC_000018262–000018285

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018273
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC31O1\3O985.D Vial: 39 Acq On 2 Jan 2002 1:45 am Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Propanone, 1-(1-methylethoxy Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

18.16 0.58 ug/1 214054 Acenaphthene-dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1-(1-methylethoxy)- 116 C6H1202 042781-12-4 25 2 2-Cycl enten-1-one, 3-amino-2-meth ill C6H9NO 069687-85-0 9 3 Aceti acid, 2-propenyl ester 100 C5H802 000591-87-7 9 4 2 -Nonanone 142 C9H180 000821-55-6 9 Abundance Scan 1429 (18.161 min): 30985.D (-) m/z 43.05 100.00% 43

57 73 5000 111 95 85 , 127 146 201 17.80 18.00 18.20 18.40 P mmmmmm TMtpmpm m/z 56.95 65.12% miz-s 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #3286:2-Propanone, 1-(1-methylethoxy)- 43

5000 18 — TTTTr 17.80 18.00 18.20 18.40 27 i 58 73 m/z 73.00 56.79% .. ।.... j. IM >. I Mip n .... । A| n l > ।।।।I (11.111 H1111.1 m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #2419: 2-Cyclopenten-1-one, 3-amino-2-methyl- 17 1—11P=Tm t hmm 7 11 IT 17.80 18.00 18.20 18.40 5000- m/z 111.10 40.03% 111 27 55 . 83 11 69 1

miz-> 10 20 30 40 50 SO' 70 80 90 100 110 120130 140 150160170180190 200 210 Abundance #63305: Acetic add, 2-propenyl ester 1 43 17.80 18.00 18.20 18.40 m/z 69.0,0 28.31% 5000

58 TpmTTTTTTT J172 27 || ......................... ...1).... 11... t.........1.... J.... 1(1......................... (1(. AfilmgamaptAtimaipi miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 17.80 18.00 18.20 18.40

30985.D GCMS1126.M Wed Jan 23 08:57:20 2002 Page 5

NYC-WTC_000018273

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NYC-WTC_000018273Source: NYC Law Department, mirrored locally

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