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GCMS analysis results for sample AD29523, Jan 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036798–000036814

Folder label: “GCMS X 12/7/01 A 1/2/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\29523.D Vial: 37 Acq On : 29 Dec 2001 12:10 am Operator: 209 GALOS Sample : GC/MS SCAN 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C: \DATABASE\NBS75K. L

Peak Number 6 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

21.04 0.53 ug/1 339768 Acenaphthene-dl0 20.57

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic acid, 4-ethoxy-, ethyl este 194 C11H1403 023676-09-7 97 2 1-Cyclopentene-1-propanoic acid, .b 168 C10H16O2 061833-30-5 46 3 Benzenepropanoic acid, 4-methoxy-, 194 C11H1403 015823-04-8 43 4 Anisyl propionate 194 C11H1403 ______ 007549-33-9 38 Abundance / Scan 1743 (21.042 min): 29523.D (-) m/z 120.95 100.00% 1

5000- 149

138 194 93 mp - 39 Hr 50 5 TTTTT 166 20.80 21.0( 21.20 21.40

m/z-> 20 30 40 76 50 60 70 80 I 103 JU r +158.4179 90 100 110 120 130 140 150 160 170 180 190 200 ■ ■ r ■ m/z 149.00 48.77% Abundance #21260: Benzoic acid, 4-ethoxy-, ethyl ester 121

149 5000- 138 20.80 21.00 21.20 21.40 194 65 93 166 m/ z 194.0 29.53% 27 | ............ 1....... I > > I f ] ■ I >> I.... 1.... 1 .1............. i .. ,....I...... I' •' 'I' • • ‘ I •'1' I " 1TTTTTTT "I" m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #14561: 1-Cyclopentene-1-propanoic acid, .beta.-methyl-. me 58 79 95 121 8000- IIT 20.80 21.00 21.20 21.40 109 6000 - m/z 138.005 26.91% 4000 150 I li 168 TT r ■" i " ’ ■ i" " i' ■" P •' • i" " p' • ‘ i pTTrpTTTyrTTTpTTTpTTTYrr^^ m/z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 'Abundance #21262: Benzenepropanoic acid, 4-methoxy-, methyl ester ............ T1T'~Tr ‘ i i i i | i i r TII 1 1 : I 121 20.80 21.00 21.20 21,40 m/ z 65 . Q 18.70% 5000 - 194

m/z-> ‘i 20 I * " ' I ’ " ‘ I " • *1 30 40 50 60 108’TTT TTTTTTTTTTTTTTCTTT Lu 134 151 163 TT‘TUT"u"tttn" " i" 70 80 90 100 110 120 130 140 150 160 170 180 190 200 TTPPMA+ 20.80 21.00 21.20 21.40

29523.D GCMS1126.M Tue Jan 08 12:09:46 2002 Page 6

NYC-WTC_000036810

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NYC-WTC_000036810Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004149

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.998

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