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GCMS analysis results for sample AD26204, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD26204 with unidentified compounds detected.

NYC-WTC_000031129–000031158

Folder label: “GCMS X 11/2/01 A 12/1/01

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NYC 9/11 Public Portal Document • Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC0401\26205.D Vial: 68 Acq On : 4 Dec 2001 10:25 am Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Misc Multipir: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 10 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 21.03 1.12 ug/1 438132 Acenaphthene-dl0 20.59

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic acid, 4-ethoxy-, ethyl este 194 C11H1403 023676-09-7 98 2 Benzenepropanoic acid, 4-methoxy-, 194 C11H1403 015823-04-8 4 3 1-Cyclopentene-l-propanoic acid, .b 168 C10H1602 061833-30-5 42 4 4-Methoxyphenylacetic acid ethyl es 194 C11H1403 014062-18-1 37 thundance Scan 1741 (21.030 min): 26205.D (-) m z 120.95 100.00% 11

149 5000 138 194 65 1 39 50 76 20.60 20.80 21.00 21.20 21.40 109 179 0 m/z 149.00 50.75% -> 20 30 40 50 60 70 80 90 100110120 130 140150 160170 180 190 200 undance #21260: Benzoic acid, 4-eUwxy-, ethyl ester 11

149 5000 138 194 20.60 20.80 21.00 21.20 21.40 m/z 194.05 31.52% 27 65 93 166

nft-> 20 30 40 50 60 70 80 90 100110120 130 140150 160170 180 190 200 .bundance #21262: Benzenepropanoic acid, 4-methoxy-, methyl ester 11

20.60 20.80 21.00 21.20 21.40 500o m/z 137.95 26.78% 194 134

-> 108 151 163 20 30 40 50 60 70 80 90 100110120 130 140150 160170 180190200 I,,,, ¼bundance #14561:1-Cyclopentene-1-propanoic acid, .beta.-methyl-, me 79 11 20.60 20.80 21.00 21.20 21.40 58 95 8000 m/z 64.95 16.41% 109 6000

4000 150 168 -> 20 30 40 50 60 70 80 90 100 110120130 140150 160170 180190 200 20.60 20.80 21.00 21.20 21.40

26205.D NP112601.M Tue Dec 04 15:58:50 2001 Page 10

NYC-WTC 000031147

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NYC-WTC_000031147Source: NYC Law Department, mirrored locally

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