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GCMS analysis results for sample AD26204, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD26204 with unidentified compounds detected.

NYC-WTC_000031129–000031158

Folder label: “GCMS X 11/2/01 A 12/1/01

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NYC 9/11 Public Portal Document • Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC0401\26205.D Vial: 68 Acq On 4 Dec 2001 10:25 am Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\1'P112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Benzoic acid, 2,6-bis[(trimeth Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 22.81 3.27 ug/1 1307170 Phenanthrene-d10 25.01 Hit# of 5 Tent Live ID MW MolForm CAS# Qual ----------------- -------------------------------------------------- 1 Benzoic acid 2,6-bis[(trimethylsil 370 C16H3004Si3 003782-85-2 32 2 Benzeneetha amine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 25 3 Benzoic a d, 2,4-bis[(trimethylsil 370 C16H3004Si3 010586-16-0 25 4 Phenethy amine, N-meth l-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 25 thundance scan 1935 (22.811 min): 26205.D (-) m z 73.00 100.00%

5000 147 355 221 281 45 117 191 401 441 22.40 22.60 22.80 23.00 23.20 249 327 m/z 355.05 34.74% -> 50 100 150 200 250 300 350 400 450 500 550 undance #51296: Benzoic acid, 2,6-bls[(trimethylsilyl)oxy]-, trimet 35

5000 22.40 22.60 2280 23.00 23.20 147 267 m/z 147.00 31.56%. 47 208 237 -> 50 100 150 200 250 300 350 400 450 500 550 bundance #74706: Benzeneethanamine, N-[(pentafluorophenyQmethylene] 355

22.40 22.60 2280 23.00 23.20 5000 m/z 221.05 23.98%

45 208 251 386 fl lz-> ndance 50 100 150 200 250 300 350 400 460 500 550 Jf #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trimet _ ITr !

22.40 2260 22.80 23.00 23.20 m/z 281.00 18.71% 5000 355 45 133 193 223 281 -> 50 100 150 200 250 300 350 400 450 500 550 2240 22.60 22.80 23.00 23.20

262b5.D NP112601.M Tue Dec 04 15:58:53 200]. Page 11

NYC-WTC 000031148

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NYC-WTC_000031148Source: NYC Law Department, mirrored locally

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