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GCMS analysis results for sample AD26204, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD26204 with unidentified compounds detected.

NYC-WTC_000031129–000031158

Folder label: “GCMS X 11/2/01 A 12/1/01

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Scanned page image, NYC-WTC_000031149
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC0401\26205.D Vial: 68 Acq On : 4 Dec 2001 10:25 am Operator: 209 GALOS Sample : 11/2 gc/ms Inst ; GC/MS 209 Misc Multipir: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

26.91 1.62 ug/l 645661 Phenanthrene-d10 25.01

Hit# of 5 Tentative ID MW MolForm CAS# Qual ------------ -------------------------------------------------------- 1 3-Isopr oxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 38 2 1-Mono noleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 36 4 . Trisi xane,. 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 28 3 4 1,1, 5,7,7,7-He tameth 1-3,3-bis(t 444 C13H4005Si6 bundance Scan 2381 (26.905 min): 26205.D(-) 038147-00-1 22 m/z 73. 00 100.00%

5000 147 221 281 327 355 26.60 26.80 27.00 27.20 45 117 191 249 401 429 m/z 147.00 37.72% —> 50 100 150 200 250 300 350 400 450 500 550 thundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(him

5000 147 26.60 26.80 27.00 27.20 m/z 281.00 22.00% 221 281 327 415 519 561 nlz—> 50 100 150 200 250 300 350 400 450 500 550 bundarice #58871:1-Monolinoleoylglycerol trimethylsityyt ether

207 26.60 26.80 27.00 27.20 5000 147 m/z 221.05 20.19% 34 103 281 • ,t, I , 11 , I I , J, , 1 ,I •I , I. 395 482 rift—> 50 100 150 200 250 300 350 400 450 500 550 ¼bundance #52459: Trlsiloxane,1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 17 26.60 26.80 27.00 27.20 m/z 206.95 9.41% 1 5000 I

100 1

26205.D NP112601.M Tue Dec 04 15:58:55 2001 Page 12

NYC-WTC 000031149

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NYC-WTC_000031149Source: NYC Law Department, mirrored locally

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