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GCMS analysis results for sample AD26204, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD26204 with unidentified compounds detected.

NYC-WTC_000031129–000031158

Folder label: “GCMS X 11/2/01 A 12/1/01

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Scanned page image, NYC-WTC_000031150
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC0401\26205.D Vial: 68 Acq On 4 Dec 2001 10:25 am Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Misc : Multipir: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 28.67 1.32 ug/l 529017 Phenanthrene-d10 25.01

Hit# of 5 Tentative ID MW MolForm CAS# Qual --------------------------------------------------------------------- 1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 28 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 27 3 Benzeneethanamine, N-E(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 12 4 Palmitic acid, 2-(trimeth lsilo )e 372 C21H44O3Si 022613-62-3 10 thunclarice Scan 2573 (28.668 min): 26205.D (-) m z 73.00 100.00%

5000 147 221 355

45 117 191 249 281. , 327 1L, , 401429 28'`0 28'6D 28.80 29.00 m/z 147.00 40.93% n/z.-> 50 100 150 200 250 300 350 400 450 500 550 bundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 44

5000 147 28.40 28.60 28.80 29.00 m/z 355.05 25.71% 221 281 327 415 519 561 rift-> 50 100 150 200 250 300 350 400 450 500 550 undance #52459: Trlsiioxane,1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet fl 17

281 28.40 28.60 28.80 29.00 5000 m/z 221.05 24.76%

369 207 249 338 -> 50 100 150 200 250 300 350 400 450 500 550 bundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 355 28.40 28.60 28.80 29.00 m/z 281.00 18.63% 5000

45 208 251 281 386 458 548 -> 50 100 150 200 250 300 350 400 450 500 550 28.40 28.60 28.80 29.00

26205.D NP112601.M Tue Dec 04 15:58:58 2001 Page 13

NYC-WTC 000031150

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NYC-WTC_000031150Source: NYC Law Department, mirrored locally

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