DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30641.D Vial: 42 Acq On : 29 Dec 2001 11:33 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 3-Isopropoxy-1,1,1,7, 7,7-hexam Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

28.66 1.39 ug/1 891599 Phenanthrene-dl0 24.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 2 N-(Trifluoracetyl)-0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 17 3 Tris(trime y1 silyl)borate 278 C9H27BO3Si3 004325-85-3 16 4 N- (Trifluoroacetyl)-0,0',0''-tris(t 481C19H34F3NO4Si3 000000-00-0 16 Abundance / Scan 2572 (28.657 min): 30641 .D (-) m/ z 73.00 100.00% 73

5000 147 221 281 355 1 ' I ' ' 1 1 1 ' 28.40 28.60 28.80 29.00 45 117. 1914 249 . [ . 327 1 401 429 ■ ''i 1 ■ — 1 - 1 -—f f i * i fi—j—j——j—।—— Titi—r m/z 147.CO 37.26% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 147 28.40 28.60 28.80 29.00 221 m/z 355.05 21.59% 281[ 327 I 415 519 561 m/z—>__ 50 100 150 200 250 300 350 400 450 500 550 Abundance 52000 N-T C 0 ris(trimethyl 73 355 28.40 28.60 28.80 29.00 5000 m/ z 221.05 21.56%

45 140 184 281 j 480 50 100 _ 150__ 200 _ 250 300 350 _ 400 450__ 500 550. Abundance #39028: Tris(trimethylsilyl)borate 73. 221 28.40 28.60 28.80 29.00 m/ z 281.00 17.14% 5000 263 133 175 | I 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 28.40 28.60 28.80 29.00

30641.D GCMS1126.M Mon Jan 28 11:14:19 2002 Page 9

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