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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004231
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2502\30651.D Vial: 35 Acq On : 25 Jan 2002 10:53 pm Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Benzoic acid, 2,4-bis[(trimeth Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

28.45 1.02 ug/1 924157 Phenanthrene-dl0 24.78

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 37 2 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 33 3 3-1 sopropoxy—1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 30 4 Trisiloxane,/ 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 30 Abundance Scan 2549 (28.448 min): 30651.D (-) m/z 73.00 100.00% 73

5000 147 - 221 281 355 28.20 28.40 28.60 28.80 45 , TT 117.4 , , 1914 191 [ 249 [ 327J fl l 1 1*1 fl‘l I 1-1-1 401 429 1 ’ 1 । 1 1 1 1 । ■ ■ ' ■ i ■ ■ m/z 147.00 33.09% m/z-> 50 100 150 200 250 300 350 400 450 500 550 [Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trimet 73

5000 355 ... M..... 28.20 28.40 28.60 28.80 45 m/z 221.0 18.25% .. .. 133 _ _ 193 223 281 ............... m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoyiglycerol trimethylsilyl ether 73

207 28.20 28.40 28.60 28.80 5000 147 m/z 355.0 16.63% 34 103 281

m/z--> 50 100 150 ' 200 250 300 350 395. .482500 . 400 450 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim ................. ............................ 73 28.20 28.40 28.60 28.80 m/z 281.00 14.11% 5000 147 221 281 327 - 415 519 561 i > ■ ■ ■ i ■ ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 28.20 28.40 28.60 28.80

30651.D GCMS1126.M Mon Jan 28 12:23:48 2002 Page 11

NYC-WTC_000004231

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NYC-WTC_000004231Source: NYC Law Department, mirrored locally

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