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GCMS blank analysis results for sample AD30643, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.

NYC-WTC_000018420–000018435

Folder label: “GCMS X 12/18/01 A 12/30/01

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Scanned page image, NYC-WTC_000018432
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC27O1\LBE.D Vial: 51 Acq On : 30 Dec 2001 8:17 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 N-(Trifluoroacetyl)-0,0*,O’‘-t Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

22.79 0.51 ug/1 212889 Acenaphthene-dl0 20.56

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

I N- (Trifluoroacetyl)-0,0‘ ,0 '’-tris(t 481 C19H34F3NO4Si3 000000-00-0 43 2 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 3 Trisiloxane, 1. ,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 37 4 N- (Trifluoracet yl)-0,0',On-tris(tri 495 C20H36F3NO4Si3 000000-00-0 37 Abundance Scan 1933 (22.789 min): LBE.D (-) m/ z 73.0,0 100.00% 73

5000 147 * 221 281 355 22.40 22.60 22.80 23.00 23.20 401 I ri 1 1 ■191, .. 251.., 327 i 45 117 — m/z 147.00 27.12% mz-> 50 100 150 200' 250 300 350 400 450 500 550 Abundance #58326: N-(Trifluoroacetyl)-O,O'.O"-tris(trfmethy(silyI)no 73 355 5000 ‘ * I • ‘ ‘ ‘ I ’ ‘ 22.40 22.60 22.80 23.00 23.20 m/z 355.0 23.84% . 45r, x 120147 193 265 ...................................... 481................. miz-> ' 50 ’•1 ■100i ■ 1 '• •150 j ■ ■ ■ • i • • ■ ■ i r 200 250 300 ‘ ‘ 350 ‘ 400 ' 450 500 ' 550 Abundance #74706: Benzeneethanamine, N-f(pentafluorophenyl)methylene] 73 355 ■ i 1 ■111 T T T 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.05 18.32%

45 208 251 281 386 458 548 m/z-> 50 100 ‘ ' 150 200 ‘ 250 300 350 466 450 “566 ‘ 550 ‘ Abundance #52459: Trisiloxane, 1,1,1.5.5,5-hexamethyl-3,3-bls[(trimet 73 147 22.40 22.60 22.80 23.00 23.20 281 m/z 281.00 13.43% 5000

369 207 249. ----- 338............... ...................... ... miz—> g 100 150 200 250 300 ‘ 350 “ 400 ‘ ' 450 " 500 ' ‘ 550 ' 22.40 22.60 22.80 23.00 23.20

LBE.D GCMS1126.M Fri Feb 01 11:32:00 2002 Page 7

NYC-WTC_000018432

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NYC-WTC_000018432Source: NYC Law Department, mirrored locally

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