NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC27O1\LBE.D Vial: 51
Acq On : 30 Dec 2001 8:17 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
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Peak Number 7 N-(Trifluoroacetyl)-0,0*,O’‘-t Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
22.79 0.51 ug/1 212889 Acenaphthene-dl0 20.56
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
I N- (Trifluoroacetyl)-0,0‘ ,0 '’-tris(t 481 C19H34F3NO4Si3 000000-00-0 43
2 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43
3 Trisiloxane, 1. ,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 37
4 N- (Trifluoracet yl)-0,0',On-tris(tri 495 C20H36F3NO4Si3 000000-00-0 37
Abundance Scan 1933 (22.789 min): LBE.D (-) m/ z 73.0,0 100.00%
73
5000
147 *
221 281 355 22.40 22.60 22.80 23.00 23.20
401
I ri 1 1 ■191, .. 251.., 327 i
45 117
— m/z 147.00 27.12%
mz-> 50 100 150 200' 250 300 350 400 450 500 550
Abundance #58326: N-(Trifluoroacetyl)-O,O'.O"-tris(trfmethy(silyI)no
73
355
5000 ‘ * I • ‘ ‘ ‘ I ’ ‘
22.40 22.60 22.80 23.00 23.20
m/z 355.0 23.84%
. 45r, x 120147 193 265 ...................................... 481.................
miz-> ' 50 ’•1 ■100i ■ 1 '• •150
j ■ ■ ■ • i • • ■ ■ i r
200 250 300 ‘ ‘ 350 ‘ 400 ' 450 500 ' 550
Abundance #74706: Benzeneethanamine, N-f(pentafluorophenyl)methylene]
73 355
■ i 1 ■111 T T T
22.40 22.60 22.80 23.00 23.20
5000 m/z 221.05 18.32%
45
208 251 281 386 458 548
m/z-> 50 100 ‘ ' 150 200 ‘ 250 300 350 466 450 “566 ‘ 550 ‘
Abundance #52459: Trisiloxane, 1,1,1.5.5,5-hexamethyl-3,3-bls[(trimet
73 147 22.40 22.60 22.80 23.00 23.20
281
m/z 281.00 13.43%
5000
369
207 249.
----- 338............... ...................... ...
miz—> g 100 150 200 250 300 ‘ 350 “ 400 ‘ ' 450 " 500 ' ‘ 550 ' 22.40 22.60 22.80 23.00 23.20
LBE.D GCMS1126.M Fri Feb 01 11:32:00 2002 Page 7
NYC-WTC_000018432
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