GC/MS calibration data for sample 30647, Dec 2001

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Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018546–000018575

Folder label: “GCMS X 12/18/01 A 12/30/01”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \HPCHEM\ 1 \DATA\DEC2 701\30706.D Vial: 54 Acq On : 30 Dec 2001 12:10 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 N-(Trifluoracetyl)-0,0',0"-tri Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.79 1.89 ug/1 1102080 Phenanthrene-dl0 24.98 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 N-(Trifluoracety1)-0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 43 2 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 3 N- (Trifluoroacetyl) -0,0' ,0' '-tris(t 481 C19H34F3NO4Si3 000000-00-0 37 4 N-(Tidfluoroacetyl)-N,0,0',0’'-tetr 553 C22H42F3NO4Si4 000000-00-0 35 Abundance Scan 1933 (22.788 mln): 30706.D (-) m/z 73.00 100.00% 73

5000 147 355 221 281 45 401 327 1 22.40 22.60 22.80 23.00 23.20 miz-> — 50 191+-244 117 100 riri—i ftIi 150 200 250 300 350 400 450 500 550 m/z 147.00 24.93% (Abundance #58807: N-(Trifluoracetyl)-O,O',O"-tris(trimethylsilyl)epin 73 355 .... . 5000 22.40 22.60 22.80 23.00 23.20 45 m/z 355.05 24.17% | 4 140 184 281 480 • ‘ I * ' • ‘ I • • ■'1 i ■ ' ■' i • • • • i ( 1 i 1 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706 Benzeneethanamine, N-Kpentafluorophenyl)methylene] 73 355 I | ! ■ ■ ■ | ■ I ! 1 |V1 .'I | ■ I I . | I I

22.40 22.60 22.80 23.00 23.20 5000 m/z 221.05 18.20%

45 | 208 251 281 386 458 548 —————————— 1111111111418* mlz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58326: N-(Trifluoroacetyl)-O,O',O"-tris(trimethylsilyl)no ..... / y..... 73 22.40 22.60 22.80 23.00 23.20 355 m/z 281.00 13.99% 5000-

45 , I , h'1111120147 193 265 ■'1'i1 ■1 ■ T11 ■111"ITTIu t 481. [ f 1 n । 1 J । • i' i i J i i > I J » » i m/z—> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20

30706.D GCMS1126.M Fri Feb 01 11:08:25 2002 Page 8

NYC-WTC_000018568

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