GC/MS calibration data for sample 30647, Dec 2001

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Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018546–000018575

Folder label: “GCMS X 12/18/01 A 12/30/01”

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Data File : C:\HPCHEM\1\DATA\DEC2 701\30706.D Vial: 54 Acq On : 30 Dec 2001 12:10 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

26.89 0.78 ug/1 452689 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane, 1, 1,1,5,5,5-hexamethyl 384 C12H36O4S15 003555-47-3 37 2 1 -Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 36 3 1,1,1,5, 7,7,7-Heptamethy1-3,3-bis(t 444 C13H40O5Si6 038147-00-1 25 4 3-Isoprcpoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 Abundance............. Scan 2380 (26.891 mln): 30706.D (-) m/z 73.00 100.00%| 73

5000 147 221 281 - 26.60 26.80 27.00 27.20 45 TTr 96 117 ,‘l l' 1'' "’“1 1 , 1911 [ 249 ... _ 327,355, , 399429 m/z 147.00 32.34% miz-> 50 100 150 200 250 300 350 400 450 (Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bls[(trimet it 73 147 281 5000 26.60 26.80 27.00 27.20 369 m/z 281.00 17.73 , - 207 249. . 338 J.......... miz-> 50 100 150 200 250 300 350 400 450 Abundance ;#58871: 1 -Monolincleoylgtycerol trimethyisilyl ether 73 ■ ■ i ■ ■ ■ • । ■ ■ ■ ■ । • ■ • ■ । ■

207 26.60 26.80 27.00 27.20 5000 147 m/z 221.05 16.10 34 103 281 1 ■ i • ■ ■ ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ • • • । z ■ । ■ ■ ■ ■ i ■ • 395.... 482 m/z-> 50 100 150 200 250 300 350 ' ■ 400 i ■ • ■ ■ 450 i ■ ■ ■ •

Abundance #56714:1,1,1,5>7.7,7-Heptamethyl-3>3-bis(trimethylslloxy)t T । f » « » । i rn i । ri 73 26.60 26.80 27.00 27.20 m/z 74.0.0 8.74 147 5000 267 355 429 45 207

miz—> I 50 100 150 ' ‘ 200 ' 250 ' ■

300 i ■ ■ • ■

350 i ■ ■ ■ •

400 I 1 ' ' 1

450 I ' 1 0 26.60 26.80 27.00 27.20

30706.D GCMS1126.M Fri Feb 01 11:08:29 2002 Page 9

NYC-WTC_000018569

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