GC/MS calibration data for sample 28323, Dec 2001

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Data File : C:\HPCHEM\l\DATA\DEC2701\28323.D Vial: 63 Acq On : 30 Dec 2001 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

21.03 1.84 ug/1 964889 Acenaphthene-dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic acid, 4-ethoxy-, ethyl este 194 C11H1403 023676-09-7 97 2 Benzenepropanoic acid, 4-methoxy-, 194 C11H1403 015823-04-8 43 3 1-Cyclopentene-1-propanoic acid, 4 1-Butanone, 4-chloro-l-(4-hydroxyph 198 C10H11C1O2 Abundance "..... X........ Scan 1741 (21.031 min): 28323.D (-) 121 .b 168 C10H16O2

m/z "s 061833-30-5 42 007150-55-2 38 100.00%

5000 149

138 194 65 93 i i -r 39 50 166 20.80 21.00 21.20 21*40 m/z-> '111 ‘111 44.7644.199.— 11'1'1 “I TII—mmuuT m/z 149.00 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 179 1 'I “ , 207 4 7.86% Abundance #69400: Benzoic acid, 4-ethoxy-, ethyl ester 121

149 5000 194 20.80 21.00 21.20 21.40 65 93 138 166 m/z 194 . s 30.34% 50 h 76 i■■■■i 4 miz-__ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 T p«»«p' * * p»• q I'''' 1 “ '

Abundance #21262; Benzenepropanoic acid, amethoy nethy aster 121

20.80 21.00 21.20 21.40 5000 m/z 137.95 25.85% 194 134 108 i 151 163 > P *>. P i rq .... p । < q 1111 p 11 q 11 r q 1111 p 111 p 111 p 111 p 111 p 111 p' 111 p 111 p r 11 p 111 p 111 p 11 mfz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #14561:1-Cyclopentene-1-propanoic acid, .beta.-methyl-, me / — TT"T ■" 1111 r ' ’ • I ' * ’ ‘ I ‘ ’ • I 79 1211 20.80 21.00 21.20 21.40 58 95 8000 m/z 65.05 20.52% 109 6000

4000 150 ............................. 1........ ........ ...... Il . 1.... ।.. n ।... ।.. >, ।.. ,,t ***,—2*****/[** , rr., ।....................................................... ।, 168 1111111111111111111111111,, ।,, ■, ।।, m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 20.80 21.00 21.20 21.40

28323.D GCMS1126.M Wed Feb 06 13:02:01 2002 Page 9

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