Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018519–000018545Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\28323.D Vial: 63 Acq On : 30 Dec 2001 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
20.28 14.93 ug/1 7832950 Acenaphthene-dl0 20.56
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 42 2 2-Hexenedioic acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 32 3 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 32 4 2-Pent oic acid, 2~[(trimethylsily 260 CllH24O3Si2 _ 055045-17-5 23 Abundance Scan 1659 (20.278 min): 28323.D (-) m/z 73.00 1 00.00% 73
5000 147 281 14 i I J » i l J » i I » 1 1 4 j I l I »' 327 20.00 20.20 20.40 20.60 —Te , 355,383 415439 45 117 , 191 221 249 — 1 [" Pithoni m/z 147.00 39.52% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane. 1,1.1,5.5,5-hexamethyl-3,3-bis[(trlmet 73 147 281 5000 20.00 20.20 20.40 20.60 ' 369 m/z 281.00 38.04% , 207 249, ------ ‘[ ‘ i • ' 338 I 1 ■ i ■ ■ ■ • i ■ • ■ ‘ i • • ■ ■ i ■ ■ 1 1 I 1 1 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #40777. 2-Hexenedicic acid, bistrimethyisil estor, (E) • 73 । i i । । i i । . । . । । । — i । r 20.00 20.20 20.40 20.60 5000 m/z 326.90 15.26% 147 45 | 112 244 273 m/z~> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3.5,5-Ws(trim 73 20.00 20.20 20.40 20.60 m/z 282.00 10.70% 5000 147
221 281 307 445 rT" u-Pemri i r r | i > > < । i r i i I 34 i i r i [ < i . / । . i » . । 415 . । ( । i । . । 519 561 1 . . । f . . ..... . ... m/z-> 50 100 150 200 250 300 350 400 450 500 550 20.00 20.20 20.40 20.60
28323.D GCMS1126.M Wed Feb 06 13:01:56 2002 Page 8
NYC-WTC_000018532
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NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018287
Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033974
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036614
Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.996
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NYC-WTC_000018416
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
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NYC-WTC_000018417
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
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NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
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NYC-WTC_000018436
Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
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NYC-WTC_000018440
Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
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