Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30708.D Vial: 49 Acq On : 30 Dec 2001 6:21 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
20.28 4.27 ug/1 2634040 Acenaphthene-dl0 20.56
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxane/ 1,1,1,5,5,5-hexamethyl 3 84 C12H3604Si5 003555-47-3 38 2 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 38 3 Octadecanoic acid. 2-[(trimethylsil 386 C22H46O3Si 056196-58-8 10 4 Phosphori % acid, 3-(ethoxyimino)-2- 429 C14H36NO6PSi3 _ 055334-96-8 10 Abundance Scan 1659 (20.276 min): 30708.D (-) m/ Z 73.0,0 100.00% 73
5000 147 281 327 45 20.00 20.20 20.40 20.60 ; 0- 117.. ..।191 2?1 251 r1 /. i f in i-| r i I 355,383 415......... m/z 147.00 36.23% m/z-? 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147
5000 281 __ JI,,..... 20.00 20.20 20.40 20.60 369 m/z 281.00 33.98% 207 I 249 I, I, 338 I , ' । । l ' m/z->___ 50__ . 100 150 __ 200 250 300 350 400 450 500 550 Abundance -043: 3 sopmpox-1.1 i 7 7 7heameh3 5,5-tis(trim 73 20.00 20.20 20.40 20.60 5000 m/z 326.90 13.29% 147 221 281 327 415..... 519 , 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52732: Octadecanoic acid, 2-[(trimethylsilyl)oxy]-> methyl 73 20.00 20.20 20.40 20.60 m/z 282.00 9.51% 5000 327 103 371 I m/z-> 1132215% 50 100 150 200 250 300 350 400 450 500 550 ............ ....... 20.00 20.20 20.40 20.60
30708.D GCMS1126.M Mon Jan 28 11:28:45 2002 Page 7
NYC-WTC_000004346
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
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